5-甲氧基-2-硝基苯甲醛合成路线 （共 41 条）
反应条件
1: 75 percent / HBF4*OEt2 / CH2Cl2 / -78 °C 2: 62 percent / H2 / Pd/C / methanol / 24 h / 20 °C / 2280 Torr View Scheme
参考文献
Islam, M. Shahidul; Brennan, Courtney; Wang, Qinwei; Hossain, M. Mahmun
Journal of Organic Chemistry, 2006 , vol. 71, # 12 p. 4675 - 4677
反应条件
1.1: 71 percent / piperidine; pyridine / 4 h / Heating 2.1: H2; AcOH / 10 percent Pd-C / 14 h / 20 °C 2.2: 88 percent / AcOH / 1 h / 70 °C View Scheme
参考文献
Iyobe; Uchida; Kamata; Hotel; Kusama; Harada
Chemical and Pharmaceutical Bulletin, 2001 , vol. 49, # 7 p. 822 - 829
反应条件
1: 69 percent / Fe; HCl 2: t-BuONO; HBr 3: CuBr View Scheme
参考文献
Tsoungas, Petros G; Searcey, Mark
Tetrahedron Letters, 2001 , vol. 42, # 37 p. 6589 - 6592
参考文献
Hodgson; Beard
Journal of the Chemical Society, 1927 , p. 2381
参考文献
Hodgson; Beard
Journal of the Chemical Society, 1927 , p. 2381
反应条件
1: acetic acid anhydride 2: iron (II)-sulfate; aqueous ammonia 3: aqueous sulfuric acid; sodium nitrite; sodium carbonate / Diazotization 4: quinoline; copper oxide-chromium oxide 5: acetic acid; aqueous HI View Scheme
参考文献
Rapson; Robinson
Journal of the Chemical Society, 1935 , p. 1533,1543
反应条件
1: permanganate 2: tin (II)-chloride; concentrated hydrochloric acid View Scheme
参考文献
Pschorr
Justus Liebigs Annalen der Chemie, 1912 , vol. 391, p. 44
反应条件
1: 74 percent / H2 / 10 percent Pd-C / 48 h / 20 °C 2: NaNO2 View Scheme
参考文献
Tsoungas, Petros G; Searcey, Mark
Tetrahedron Letters, 2001 , vol. 42, # 37 p. 6589 - 6592
反应条件
1: 88 percent / NH2OH*HCl; MgSO4; p-TsOH*H2O / toluene / 15 h / Heating 2: 56 percent / SnCl2*H2O / methanol / 3 h / 70 °C View Scheme
参考文献
Norris,R.K.; Sternhell,S.
Australian Journal of Chemistry, 1972 , vol. 25, p. 2621 - 2629
反应条件
2: ferrosulfate; ammonia 3: Behandeln mit Kupferbromuer.Diazotization View Scheme
参考文献
Pschorr
Justus Liebigs Annalen der Chemie, 1912 , vol. 391, p. 44
