(6E)-6-[(羟基-苯基氨基)亚甲基]环己-2,4-二烯-1-酮合成路线 (共 15 条)
反应条件
Lawesson's reagent in benzene T=20°C; 0.5 h;
参考文献
Jorgensen, K. A.; Shabana, R.; Scheibye, S.; Lawesson, S.-O.
Bulletin des Societes Chimiques Belges, 1980 , vol. 89, # 3 p. 247 - 254
参考文献
Jolles; Krugliakoff
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1930 , vol. <6>11, p. 197,201
反应条件
in ethanol 0.166667 h; RefluxGreen chemistry;
参考文献
Kumar, Dhruva; Suresh; Sandhu, Jagir S.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 8 p. 1157 - 1160
反应条件
in benzene to benzene soln. of nitrone of salicylaldehyde added (C6H4O2)BOC4H9 (molar ratio 1:1), refluxed for 30 min; concd. in vac., added petroleum ether, ppt. washed with ether, dried, elem. anal.;
参考文献
Kliegel, Wolfgang; Nanninga, Dierk
Journal of Organometallic Chemistry, 1983 , vol. 243, # 4 p. 373 - 386
反应条件
potassium in tetrahydrofuran 10 h; and 15 h; Product distributionMechanism;
参考文献
Canadian Journal of Chemistry, , vol. 65, p. 2039 - 2049