1: 3-methylbenzoic acid chloride With morpholine; diisobutylaluminium hydride in tetrahydrofuran; hexane T=0°C; 0.166667 h; Inert atmosphere; 2: n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.166667 h;

1: in toluene 2: With sulfuric acid in toluene

Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran 24 h; Ambient temperature; Yield given. Yields of byproduct given;

palladium; triphenylphosphine in tetrahydrofuran T=50°C; Negishi Coupling; 6 h; Inert atmosphereGreen chemistry; Catalytic behavior;

diethyl ether