2H-1,3-苯并噁嗪-2,4(3H)-二酮合成路线 (共 44 条)
反应条件
in ethanol; water T=35 - 37°C; 18 h; rat liver microsomes, pH 7.4; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 53, # 17 p. 4112 - 4114
反应条件
in ethanol; water T=35 - 37°C; 18 h; rat liver microsomes, pH 7.4; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 53, # 17 p. 4112 - 4114
反应条件
in toluene 4 h; Heating;
参考文献
Zaleska; Lis
Pharmazie, 1995 , vol. 50, # 2 p. 150 - 151
参考文献
Ried, Walter; Erle, Hanns-Eberhard
Chemische Berichte, 1982 , vol. 115, # 4 p. 1662 - 1664
反应条件
1: 59 percent / triethylamine / toluene / 20 h / Heating 2: 36 percent / conc. HCl / ethanol / 17 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, p. 1159 - 1167
反应条件
1: CHCl3 / 0.25 h / 0 - 24 °C 2: triethylamine / CHCl3 / 72 h / 23 °C View Scheme
参考文献
Tetrahedron, , vol. 50, # 22 p. 6549 - 6558
反应条件
in dichloromethane 2 h; Ambient temperature;
参考文献
Geffken, Detlef
Liebigs Annalen der Chemie, 1981 , # 8 p. 1513 - 1514
反应条件
1: 43 percent / 5 h / 150 - 170 °C 2: 41 percent / conc. HCl / ethanol / 1.) 15 min heated on a steam bath; 2.) 2 days, room temperature. View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, p. 1159 - 1167
反应条件
1: 75 percent / triethylamine / toluene / 46 h / Heating 2: 44 percent / conc. HCl / ethanol / 1.) reflux, 1.5 h; 2.) room temp., 2 d. View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, p. 1159 - 1167
反应条件
1: 0.40 g / 150 - 190 °C 2: 36 percent / conc. HCl / ethanol / 17 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 20, p. 1159 - 1167