(+)-柠檬烯 1,2-环氧合成路线 (共 24 条)
反应条件
dihydrogen peroxide in benzonitrile; acetonitrile; Sec-butyl alcohol T=65°C; 6 h; Reagent/catalyst;
参考文献
Dalton Transactions, , vol. 42, # 15 p. 5546 - 5553
反应条件
glucose-6-phosphate dehydrogenase; CYP102A1 cytochrome-P450 monooxygenase A328V/L437A mutant; tris(hydroxymethyl)methylamine hydrochloride; β-D-glucose-6-phosphate sodium salt; NADPH in water; dimethyl sulfoxide T=30°C; 2 h; Enzymatic reaction;
参考文献
ChemBioChem, , vol. 12, # 9 p. 1346 - 1351
反应条件
tert.-butylhydroperoxide; [MoO2Cl{HC(3,5-Me2pz)3}]BF4 in decane
参考文献
Inorganic Chemistry, , vol. 50, # 8 p. 3490 - 3500
反应条件
dihydrogen peroxide; sodium hydrogencarbonate; benzonitrile in methanol 96 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Australian Journal of Chemistry, , vol. 39, # 3 p. 441 - 446
反应条件
isopropyl alcohol in toluene T=110°C; 24 h; Inert atmosphere;
参考文献
Mitsudome, Takato; Noujima, Akifumi; Mikami, Yusuke; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
Angewandte Chemie - International Edition, 2010 , vol. 49, # 32 p. 5545 - 5548
反应条件
sulfur dioxide; epoxysulfonyl fluoride in carbon disulfide Yield given. Yields of byproduct given;
参考文献
Baig, Mirza Azam; Banthorpe, Derek V.; Carr, Graham; Whittaker, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1981 - 1986
反应条件
sulfur dioxide; epoxysulfonyl fluoride in carbon disulfide Yield given. Yields of byproduct given;
参考文献
Baig, Mirza Azam; Banthorpe, Derek V.; Carr, Graham; Whittaker, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1981 - 1986
反应条件
sulfur dioxide; epoxysulfonyl fluoride in carbon disulfide Yield given. Yields of byproduct given;
参考文献
Baig, Mirza Azam; Banthorpe, Derek V.; Carr, Graham; Whittaker, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1981 - 1986
反应条件
sulfur dioxide; epoxysulfonyl fluoride in carbon disulfide Yield given. Yields of byproduct given;
参考文献
Baig, Mirza Azam; Banthorpe, Derek V.; Carr, Graham; Whittaker, David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 1981 - 1986
反应条件
1.1: (PhSe)2; NaBH4 / 0 °C 1.2: 28 percent / H2O2 / 0 °C 2.1: 20 percent / BF3*Et2O; MgSO4; NaHCO3 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 12 p. 3698 - 3702