1-叠氮-1-脱氧-β-D-吡喃葡萄糖苷合成路线 （共 21 条）
反应条件
sodium azide in water T=30°C; var. nucleophiles and their conc.; Rate constantMechanism;
参考文献
Journal of the American Chemical Society, , vol. 113, # 21 p. 7951 - 7958
反应条件
1: 77.3 percent / NaN3 / dimethylformamide / 3.5 h / 50 °C 2: 99 percent / NaOMe / 1,2-dimethoxy-ethane; methanol / 1.5 h / 15 °C View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 47, # 2 p. 281 - 285
反应条件
1: 93 percent / NaN3; tetrabutylammonium hydrogen sulfate; NaHCO3 / CH2Cl2; H2O / 3 h / 20 °C 2: 90 percent / KOH / methanol; H2O / 3 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 48, # 23 p. 3953 - 3957
反应条件
1: 79 percent / NaN3 / hexamethylphosphoric acid triamide / 18 h / 20 °C 2: MeONa / methanol / 18 h / 20 °C View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 47, # 2 p. 281 - 285
反应条件
1: tin(IV) chloride; trimethylsilylazide / dichloromethane / 20 °C 2: sodium methylate; methanol View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 23, # 2 p. 455 - 459
参考文献
Chemische Berichte, , vol. 88, p. 475,479
反应条件
sodium azide; Aspergillus niger ASKU28 glycoside hydrolase family 3 β-glucosidase D487A mutant in aq. buffer T=40°C; pH=6.0; 0.166667 h; Enzymatic reaction; Kinetics; ConcentrationReagent/catalyst;
参考文献
Biochimica et Biophysica Acta - General Subjects, , vol. 1830, # 3 p. 2739 - 2749
反应条件
sodium azide; Aspergillus niger ASKU28 glycoside hydrolase family 3 β-glucosidase E490A mutant in aq. buffer T=40°C; pH=6.0; Enzymatic reaction; Kinetics; Concentration;
参考文献
Biochimica et Biophysica Acta - General Subjects, , vol. 1830, # 3 p. 2739 - 2749
反应条件
sodium azide; Sulfolobus solfatarius β-glucosidase SSO1353 D462 mutant T=65°C; pH=5.5; aq. bufferEnzymatic reaction; Kinetics;
参考文献
Journal of Biological Chemistry, , vol. 285, # 27 p. 20691 - 20703
反应条件
palladium on activated charcoal; hydrogen in methanol
参考文献
de Barros, Andre Luis Branco; Cardoso, Valbert Nascimento; Mota, Luciene das Gracas; Leite, Elaine Amaral; Oliveira, Monica Cristina de; Alves, Ricardo Jose
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 9 p. 2497 - 2499
