反应条件
1: 1.) BuLi / 1) THF, -70 deg C, 30 min; 2) THF, room temperature, 1 h
2: 96 percent / sodium perborate tetrahydrate / acetic acid / 3 h / 50 °C
3: 1.) BuLi / 1) hexane, THF, -70 deg C, 30 min; 2) THF, hexane, -70 deg C --> room temperature 2 h
4: 5 percent Chromat. / Ni(acac)2 / tetrahydrofuran; diethyl ether / 24 h / 40 °C
View Scheme
参考文献
Clayden, Jonathan; Julia, Marc
Journal of the Chemical Society, Chemical Communications, 1993 , # 22 p. 1682 - 1683
