2-(2-氨基乙基)苯酚合成路线 （共 24 条）
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 2 h; Inert atmosphere; 2: With water in tetrahydrofuran T=0°C; Inert atmosphere;
参考文献
Hellal, Malik; Singh, Shambhavi; Cuny, Gregory D.
Tetrahedron, 2012 , vol. 68, # 6 p. 1674 - 1681
反应条件
boron tribromide in 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran
参考文献
VIFOR (INTERNATIONAL) AG
Patent: US2012/202806 A1, 2012 ;
反应条件
sodium azide in various solvent(s) 0.75 h;
参考文献
Rastetter, William H.; Nummy, Larry J.
Journal of Organic Chemistry, 1980 , vol. 45, # 16 p. 3149 - 3155
反应条件
lithium perchlorate in benzene-d6 T=55°C; 0.75 h;
参考文献
Journal of Organic Chemistry, , vol. 45, # 16 p. 3149 - 3155
反应条件
hydrogenchloride; palladium 10 on activated carbon; hydrogen in ethanol P=2068.65 Torr; 10 h;
参考文献
Journal of Medicinal Chemistry, , vol. 51, # 18 p. 5506 - 5521
反应条件
1: 84 percent / K2CO3 / ethanol / Heating 2: 91 percent / NH4OAc / acetic acid / 1.5 h / Heating 3: 1.) LAH, 2.) H2 / 2.) Pd/C / 1.) THF, room temperature, 3 h, 2.) EtOH, 3.8 atm, 24 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 1 p. 223 - 227
反应条件
1: 91 percent / NH4OAc / acetic acid / 1.5 h / Heating 2: 1.) LAH, 2.) H2 / 2.) Pd/C / 1.) THF, room temperature, 3 h, 2.) EtOH, 3.8 atm, 24 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 1 p. 223 - 227
反应条件
dimethylsulfide borane complex in tetrahydrofuran
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS
Patent: WO2008/134474 A2, 2008 ;
Location in patent: Page/Page column 73 ;
反应条件
1: (i) NH4OAc, (ii) LiAlH4, Et2O 2: aq. HCl / 160 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 86, p. 3075 - 3084
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=20°C; Inert atmosphere;
参考文献
Journal of Medicinal Chemistry, , vol. 54, # 24 p. 8305 - 8320
