iodosylbenzene; 1-butylpyridinium tetrafluoroborate; [MnIIIT(N-Me-4-Py)P][PF6]5 T=30°C; 4 h; in open air; Title compound not separated from byproducts.;
1: With bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; josiphos in 1,2-dichloro-ethane 24 h; 2: With sodium hydroxide; dihydrogen peroxide in diethyl ether T=0 - 20°C; 2 h; Title compound not separated from byproducts;
参考文献
Crudden, Cathleen M.; Hleba, Yonek B.; Chen, Austin C.
Journal of the American Chemical Society, 2004 , vol. 126, # 30 p. 9200 - 9201
