您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴苯乙烯
合成路线
（共 88 条）
2039-88-5
2-溴苯乙烯
→
反应条件
918867-78-4
反应条件
1.1: diethyl zinc; trifluoroacetic acid / CH2Cl2; hexane / 20 h / cooling 1.2: 93 percent / CH2Cl2; hexane / 0.5 h / cooling 2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / cooling 2.2: 60 percent / hexane; tetrahydrofuran / 0.5 h / 20 °C 3.1: thionyl chloride / 1 h / 65 °C 4.1: 85 percent / triethylamine / CH2Cl2 5.1: 43 percent / benzoquinone / PdCl2(MeCN)2 / dioxane / 12 h / 80 °C View Scheme
参考文献
He, Zhi; Yudin, Andrei K.
Organic Letters, 2006 , vol. 8, # 25 p. 5829 - 5832
2039-88-5
2-溴苯乙烯
+
104-94-9
对甲氧基苯胺
→
反应条件
93597-01-4
1-(4-甲氧基苯基)吲哚
反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; sodium tert-pentoxide / 1,4-dioxane / 12 h / 110 °C / |Inert atmosphere 2: Ru(bpz)3(PF6)2 / acetonitrile / 12 h / 20 °C / |Irradiation; |Inert atmosphere View Scheme
参考文献
Maity, Soumitra; Zheng, Nan
Angewandte Chemie - International Edition, 2012 , vol. 51, # 38 p. 9562 - 9566
2039-88-5
2-溴苯乙烯
→
反应条件
96557-30-1
2-溴苯乙醛
反应条件
water; palladium dichloride in N,N-dimethyl-formamide T=20°C; Wacker reaction; 5 h;
参考文献
Wright, Joseph A.; Gaunt, Matthew J.; Spencer, Jonathan B.
Chemistry - A European Journal, 2006 , vol. 12, # 3 p. 949 - 955
95-16-9
苯并噻唑
+
2039-88-5
2-溴苯乙烯
→
反应条件
22901-00-4
2-(2-溴苯基)苯并噻唑
反应条件
Iron (III) nitrate nonahydrate; oxygen; [(t-Bu)3PH]BF4 in water; dimethyl sulfoxide T=120°C; 24 h; Sealed tubeGreen chemistry;
参考文献
Khemnar, Ashok B.; Bhanage, Bhalchandra M.
RSC Advances, 2014 , vol. 4, # 18 p. 8939 - 8942
187737-37-7
+
2039-88-5
2-溴苯乙烯
→
反应条件
4773-82-4
反应条件
palladium diacetate; tetrabutylammomium bromide; potassium hydrogencarbonate; lithium chloride in various solvent(s) T=100°C; P=6000.5 Torr; 96 h;
参考文献
Braese, Stefan; Ruemper, Joerg; Voigt, Katharia; Albecq, Stephane; Thurau, Gert; et al.
European Journal of Organic Chemistry, 1998 , # 4 p. 671 - 678
2039-88-5
2-溴苯乙烯
→
反应条件
50564-91-5
反应条件
1.1: diethyl zinc; trifluoroacetic acid / CH2Cl2; hexane / 20 h / cooling 1.2: 93 percent / CH2Cl2; hexane / 0.5 h / cooling 2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / cooling 2.2: 60 percent / hexane; tetrahydrofuran / 0.5 h / 20 °C 3.1: thionyl chloride / 1 h / 65 °C 4.1: 95 percent / triethylamine / CH2Cl2 5.1: 10 percent / CuCl2; benzoquinone / PdCl2 / dioxane / 12 h / 80 °C View Scheme
参考文献
He, Zhi; Yudin, Andrei K.
Organic Letters, 2006 , vol. 8, # 25 p. 5829 - 5832
2039-88-5
2-溴苯乙烯
→
反应条件
50564-92-6
反应条件
1.1: diethyl zinc; trifluoroacetic acid / CH2Cl2; hexane / 20 h / cooling 1.2: 93 percent / CH2Cl2; hexane / 0.5 h / cooling 2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / cooling 2.2: 60 percent / hexane; tetrahydrofuran / 0.5 h / 20 °C 3.1: thionyl chloride / 1 h / 65 °C 4.1: 79 percent / triethylamine / CH2Cl2 5.1: 6 percent / benzoquinone / PdCl2(MeCN)2 / dioxane / 12 h / 80 °C View Scheme
参考文献
He, Zhi; Yudin, Andrei K.
Organic Letters, 2006 , vol. 8, # 25 p. 5829 - 5832
2039-88-5
2-溴苯乙烯
→
反应条件
53890-83-8
反应条件
1.1: diethyl zinc; trifluoroacetic acid / CH2Cl2; hexane / 20 h / cooling 1.2: 93 percent / CH2Cl2; hexane / 0.5 h / cooling 2.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / cooling 2.2: 60 percent / hexane; tetrahydrofuran / 0.5 h / 20 °C 3.1: thionyl chloride / 1 h / 65 °C 4.1: 75 percent / triethylamine / CH2Cl2 5.1: 12 percent / benzoquinone / PdCl2(MeCN)2 / dioxane / 12 h / 80 °C View Scheme
参考文献
He, Zhi; Yudin, Andrei K.
Organic Letters, 2006 , vol. 8, # 25 p. 5829 - 5832
75-21-8
环氧乙烷
+
2039-88-5
2-溴苯乙烯
→
反应条件
55488-94-3
反应条件
1: trans-2-bromostyrene With n-butyllithium in tetrahydrofuran T=-78°C; 2: oxirane in tetrahydrofuran
参考文献
Fustero, Santos; Rodriguez, Elsa; Lazaro, Ruben; Herrera, Lidia; Catalan, Silvia; Barrio, Pablo
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 6 p. 1058 - 1064
2039-88-5
2-溴苯乙烯
+
72824-04-5
烯丙基硼酸频哪醇酯
→
反应条件
反应条件
Grubb's 2nd generation catalyst in dichloromethane olefin cross-metathesis; 12 h; Heating; Title compound not separated from byproducts;
参考文献
Morrill, Christie; Grubbs, Robert H.
Journal of Organic Chemistry, 2003 , vol. 68, # 15 p. 6031 - 6034
首页
上一页
1
...
5
6
7
8
9
下一页
末页
到第
页
确定
