1-(6-甲氧基-3,4-二氢-2H-苯并吡喃-3-基)甲胺合成路线 (共 3 条)
反应条件
lithium aluminium tetrahydride in diethyl ether Reduction; 5 h; Heating;
参考文献
Viaud; Mamai; Guerin; Bennejean; Renard; Delagrange; Guardiola-Lemaitre; Howell; Guillaumet
Pharmacy and Pharmacology Communications, 1998 , vol. 4, # 1 p. 47 - 56
反应条件
1: 79 percent / DABCO / 20 h / 50 °C 2: 92 percent / H2 / 10 percent Pd-C / methanol / 22 h / 2585.74 Torr / room t. 3: 76 percent / LiAlH4 / diethyl ether / 5 h / Heating View Scheme
参考文献
Viaud; Mamai; Guerin; Bennejean; Renard; Delagrange; Guardiola-Lemaitre; Howell; Guillaumet
Pharmacy and Pharmacology Communications, 1998 , vol. 4, # 1 p. 47 - 56
反应条件
1: 92 percent / H2 / 10 percent Pd-C / methanol / 22 h / 2585.74 Torr / room t. 2: 76 percent / LiAlH4 / diethyl ether / 5 h / Heating View Scheme
参考文献
Viaud; Mamai; Guerin; Bennejean; Renard; Delagrange; Guardiola-Lemaitre; Howell; Guillaumet
Pharmacy and Pharmacology Communications, 1998 , vol. 4, # 1 p. 47 - 56