2,4,6-三甲基苯丙酮合成路线 (共 20 条)
反应条件
aluminium trichloride in dichloromethane T=0°C;
参考文献
Pinkus, George A.; Sabesan, Arunachalam
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 473 - 477
反应条件
aluminium trichloride 5 h; Ambient temperature;
参考文献
Roberts, Royston M.; El-Khawaga, Ahmed M.; Roengsumran, Sophon
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3180 - 3183
反应条件
[Cp*Ru(CNCH3)3]+PF6-; potassium carbonate in acetonitrile 1 h; Inert atmosphereReflux;
参考文献
Bouziane, Asmae; Carboni, Bertrand; Bruneau, Christian; Carreaux, Francois; Renaud, Jean-Luc
Tetrahedron, 2008 , vol. 64, # 51 p. 11745 - 11750
反应条件
ethanol; nickel T=20°C; Hydrogenation;
参考文献
Fuson; McKeever
Journal of the American Chemical Society, 1940 , vol. 62, p. 2088,2090
反应条件
aluminium trichloride in carbon disulfide 0.5 h; Heating;
参考文献
Heathcock, Clayton H.; Buse, Charles T.; Kleschick, William A.; Pirrung, Michael C.; Sohn, John E.; Lampe, John
Journal of Organic Chemistry, 1980 , vol. 45, # 6 p. 1066 - 1081
反应条件
hafnium triflate; lithium perchlorate in nitromethane 6 h; Ambient temperature;
参考文献
Hachiya, Iwao; Moriwaki, Mitsuhiro; Kobayashi, Shu
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 7 p. 2053 - 2060
反应条件
1: AlCl3; carbon disulfide / 10 °C 2: ethanol; Raney nickel / 20 °C / Hydrogenation View Scheme
参考文献
Fuson; McKeever
Journal of the American Chemical Society, 1940 , vol. 62, p. 2088,2090
反应条件
2: dibutyl ether / anschliessendes Behandeln mit verd. wss. Saeure View Scheme
参考文献
Fuson; Bottorff; Speck
Journal of the American Chemical Society, 1942 , vol. 64, p. 1450
Journal of the American Chemical Society, 1944 , vol. 66, p. 2135
反应条件
anhydrous butyl ether anschliessendes Behandeln mit verd. wss. Saeure;
参考文献
Fuson; Bottorff; Speck
Journal of the American Chemical Society, 1942 , vol. 64, p. 1450
Journal of the American Chemical Society, 1944 , vol. 66, p. 2135
参考文献
Fuson et al.
Journal of the American Chemical Society, 1944 , vol. 66, p. 1873