1-(4-甲氧基苯基)-2,2-二甲基丙烷-1-酮合成路线 (共 29 条)
反应条件
triethylamine; selenium monobromide in dichloromethane
参考文献
Okuma, Kentaro; Kubo, Kento; Yokomori, Yoshinobu
Heterocycles, 2003 , vol. 60, # 2 p. 299 - 302
参考文献
Baciocchi, Enrico; Bietti, Massimo; Putignani, Lorenza; Steenken, Steen
Journal of the American Chemical Society, 1996 , vol. 118, # 25 p. 5952 - 5960
反应条件
dipotassium peroxodisulfate; water; tert-butyl alcohol
T=25°C; Oxidation; pH=4; γ-Irradiation; Title compound not separated from byproducts;
参考文献
Baciocchi, Enrico; Bietti, Massimo; Steenken, Steen
Chemistry - A European Journal, 1999 , vol. 5, # 6 p. 1785 - 1793
反应条件
AZADO; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane
T=20°C; 4 h;
参考文献
Hamada, Shohei; Furuta, Takumi; Wada, Yoshiyuki; Kawabata, Takeo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 31 p. 8093 - 8097
Angew. Chem., 2013 , vol. 125, # 31 p. 8251 - 8255,5
反应条件
C10H16NO5; potassium carbonate; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane
T=20°C;
参考文献
Hamada, Shohei; Furuta, Takumi; Wada, Yoshiyuki; Kawabata, Takeo
Angewandte Chemie - International Edition, 2013 , vol. 52, # 31 p. 8093 - 8097
Angew. Chem., 2013 , vol. 125, # 31 p. 8251 - 8255,5
反应条件
trifluoroacetic acid
5 h; Heating;
参考文献
Keumi, Takashi; Morita, Toshio; Shimada, Takanobu; Teshima, Naomi; Kitajima, Hidehiko; Prakash, G. K. Surya
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 847 - 852
反应条件
in diethyl ether
T=-78°C; Reflux;
参考文献
Jennings, W. Brian; O'Connell, Niamh; Malone, John F.; Boyd, Derek R.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 32 p. 5278 - 5291
反应条件
9,10-anthracenedicarbonitrile; oxygen in acetonitrile
T=5 - 10°C; 0.333333 h; Irradiation;
参考文献
Lykakis, Ioannis N.; Lestakis, Stellios; Orfanopoulos, Michael
Tetrahedron Letters, 2003 , vol. 44, # 33 p. 6247 - 6251
反应条件
1: 60 percent / diselenium dibromide; triethylamine / CH2Cl2
2: 28 percent / m-CPBA / 20 °C
View Scheme
参考文献
Okuma, Kentaro; Kubo, Kento; Yokomori, Yoshinobu
Heterocycles, 2003 , vol. 60, # 2 p. 299 - 302
参考文献
Tsatsas,G.; Cotakis,G.
Bulletin de la Societe Chimique de France, 1970 , p. 3609 - 3616