3-(4-甲氧基苯基)丙醛合成路线 （共 75 条）
反应条件
tetrabutyl-ammonium chloride; palladium diacetate; sodium hydrogencarbonate in N,N-dimethyl-formamide T=50°C; Heck Reaction; 7 h; Schlenk techniqueInert atmosphere;
参考文献
Arkivoc, , vol. 2012, # 3 p. 297 - 311
反应条件
[rhodium(I)(carbonyl)2(acetylacetonate)]; hydrogen; (R,S)-Binaphos in benzene T=60°C; P=38000 Torr; 34 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Nozaki, Kyoko; Sakai, Nozomu; Nanno, Tetsuo; Higashijima, Takanori; Mano, Satoshi; Horiuchi, Toshihide; Takaya, Hidemasa
Journal of the American Chemical Society, 1997 , vol. 119, # 19 p. 4413 - 4423
反应条件
triethylsilane; palladium on activated charcoal in tetrahydrofuran T=20°C; Fukuyama reduction; 2 h; Product distribution; Further Variations:SolventsCatalyststime;
参考文献
Kimura, Mayumi; Seki, Masahiko
Tetrahedron Letters, 2004 , vol. 45, # 16 p. 3219 - 3223
反应条件
Rh(acac)2(CO)2; 3,3',5,5'-tetratolylbiphenyl-2,2',6,6'-tetrakis(dipyrrolylphosphinite); hydrogen in toluene T=80°C; P=7600.51 Torr; 12 h; Autoclave; regioselective reaction;
参考文献
Organic Letters, , vol. 11, # 1 p. 241 - 244
反应条件
1: With 1H-imidazole; N-(trimethylsilyl)-imidazole in toluene T=55°C; McFadyen-Stevens Reaction; 2: With citric acid in methanol T=20°C; McFadyen-Stevens Reaction;
参考文献
Iwai, Yuri; Ozaki, Takashi; Takita, Ryo; Uchiyama, Masanobu; Shimokawa, Jun; Fukuyama, Tohru
Chemical Science, 2013 , vol. 4, # 3 p. 1111 - 1119
反应条件
4-(N,N-dimethlyamino)pyridine; formic acid; Rh6(CO)12; carbon monoxide in tetrahydrofuran T=30°C; P=3800 Torr; 5 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 7 p. 2378 - 2381
反应条件
sodium hydrogencarbonate; palladium diacetate in water T=60°C; 0.25 h;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
Synthesis, 2006 , # 20 p. 3443 - 3452
反应条件
mercury dichloride in water; acetonitrile
参考文献
Dondoni, Alessandro; Fantin, Giancarlo; Fogagnolo, Marco; Medici, Alessandro; Pedrini, Paola
Tetrahedron, 1988 , vol. 44, # 7 p. 2021 - 2032
反应条件
N,N-dicyclohexylmethylamine; potassium carbonate; bis(dibenzylideneacetone)-palladium(0); cataCXium PIntB in N,N-dimethyl-formamide T=100°C; 0.5 h; Molecular sieveInert atmosphere;
参考文献
Organic Letters, , vol. 13, # 20 p. 5456 - 5459
反应条件
methanol; formic acid; water; silica gel; palladium dichloride 0.9 h; Irradiationmicrowave;
参考文献
Advanced Synthesis and Catalysis, , vol. 348, # 3 p. 354 - 360
