3-(4-甲氧基苯基)丙醛合成路线 （共 75 条）
反应条件
iodine; potassium carbonate in toluene Reflux;
参考文献
Chemistry - A European Journal, , vol. 17, # 48 p. 13502 - 13509
反应条件
1: 79 percent / sulfuric acid / 4 h 2: 94 percent / LiAlH4 / tetrahydrofuran / 16 h / Heating 3: H2CrO4 on SiO2 / diethyl ether / 0.25 h View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 44, # 2 p. 372 - 375
反应条件
1: 97 percent / acetonitrile / 24 h / Heating 2: 84 percent / sodium borohydride / methanol / -10 °C 3: 70 percent / HgCl2 / acetonitrile; H2O View Scheme
参考文献
Tetrahedron, , vol. 44, # 7 p. 2021 - 2032
反应条件
1: 84 percent / sodium borohydride / methanol / -10 °C 2: 70 percent / HgCl2 / acetonitrile; H2O View Scheme
参考文献
Tetrahedron, , vol. 44, # 7 p. 2021 - 2032
反应条件
sulfuric acid in ethanol
参考文献
Bulletin de la Societe Chimique de France, , p. 1194 - 1198
反应条件
water T=41°C; also for the reactions in presence of nucleophiles; Rate constantMechanism;
参考文献
Journal of the American Chemical Society, , vol. 111, # 20 p. 7900 - 7909
反应条件
in water T=25°C; rate of hydrolysis vs N3(1-) concentration; Rate constantMechanism;
参考文献
Journal of the American Chemical Society, , vol. 110, p. 3677 - 3679
反应条件
1: 94 percent / LiAlH4 / tetrahydrofuran / 16 h / Heating 2: H2CrO4 on SiO2 / diethyl ether / 0.25 h View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 44, # 2 p. 372 - 375
反应条件
1: 59 percent / lithium aluminium hydride / diethyl ether 2: 62 percent / pyridine 3: 80 percent / lithium bromide / acetone / 24 h / Ambient temperature 4: magnesium (from magnesium chloride and potassium metal, 3-(4-methoxyphenyl)propanal / tetrahydrofuran 5: 74 percent / pyridinium chlorochromate / CH2Cl2 / 4.5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 614 - 622
反应条件
1: 62 percent / pyridine 2: 80 percent / lithium bromide / acetone / 24 h / Ambient temperature 3: magnesium (from magnesium chloride and potassium metal, 3-(4-methoxyphenyl)propanal / tetrahydrofuran 4: 74 percent / pyridinium chlorochromate / CH2Cl2 / 4.5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 614 - 622
