3-(4-甲氧基苯基)丙醛合成路线 (共 75 条)
反应条件
sand unter vermindertem Druck;
参考文献
Journal of the Chemical Society, , p. 1571
反应条件
1: phosphorus (V)-oxide; xylene 2: HCl; SnCl2; diethyl ether / und Erwaermen des Reaktionsprodukts mit wss.Na2CO3-Loesung View Scheme
参考文献
Journal of the Chemical Society, , p. 1571
反应条件
NaY zeolite in dichloromethane Friedel-Crafts alkylation; 12 h; Heating; Product distribution; Further Variations:Catalysts;
参考文献
Chemistry Letters, , vol. 34, # 5 p. 708 - 709
反应条件
1: 94 percent / TiCl4*2THF; Zn / tetrahydrofuran / 4 h / Heating 2: aq. LiOH / tetrahydrofuran; methanol / 96 h / 20 °C View Scheme
参考文献
Xiao, Xiangshu; Antony, Smitha; Kohlhagen, Glenda; Pommier, Yves; Cushman, Mark
Journal of Organic Chemistry, 2004 , vol. 69, # 22 p. 7495 - 7501
反应条件
1: tetra-n-butylammonium tribromide / acetonitrile / 0.5 h / 20 °C 2: ethanol / 1 h / Reflux View Scheme
参考文献
DEVELOPMENT CENTER FOR BIOTECHNOLOGY
Patent: US2012/172374 A1, 2012 ;
反应条件
pyrrolidine in N,N-dimethyl-formamide T=115°C; 6 h; Inert atmosphere;
参考文献
Colbon, Paul; Ruan, Jiwu; Purdie, Mark; Mulholland, Keith; Xiao, Jianliang
Organic Letters, 2011 , vol. 13, # 20 p. 5456 - 5459
反应条件
magnesium in tetrahydrofuran
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 614 - 622
反应条件
manganese(IV) oxide; benzyl-methyl-amine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in tetrahydrofuran T=20°C; 6 h;
参考文献
Hayashi, Yujiro; Itoh, Takahiko; Ishikawa, Hayato
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3661 - 3669
反应条件
manganese(IV) oxide; benzyl-methyl-amine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in tetrahydrofuran T=20°C; 6 h;
参考文献
Hayashi, Yujiro; Itoh, Takahiko; Ishikawa, Hayato
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3661 - 3669
反应条件
ammonium hydroxide T=25°C; 7 h;
参考文献
Telvekar, Vikas N.; Rane, Rajesh A.; Namjoshi, Tejal V.
Synthetic Communications, 2010 , vol. 40, # 4 p. 494 - 497