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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-溴苯腈
合成路线
（共 287 条）
→
反应条件
72093-43-7
4-氟-4-甲基-1,1-联苯
+
114772-53-1
2-氰基-4'-甲基联苯
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; Negishi cross-coupling; 48 h; Inert atmosphere;
参考文献
Dong, Zhi-Bing; Manolikakes, Georg; Shi, Lei; Knochel, Paul; Mayr, Herbert
Chemistry - A European Journal, 2010 , vol. 16, # 1 p. 248 - 253
2042-37-7
2-溴苯腈
→
反应条件
7254-06-0
3-氯-9H-芴-9-酮
反应条件
1: palladium diacetate; potassium carbonate / water; N,N-dimethyl-formamide / 1 h / 20 °C 2: IPy2BF4; tetrafluoroboric acid / dichloromethane; diethyl ether / 24 h / -70 °C 3: palladium diacetate; triphenylphosphine; triethylamine / water; N,N-dimethyl-formamide / 16 h / 130 °C / |Inert atmosphere View Scheme
参考文献
Sarkar, Satinath; Jana, Manoranjan; Narender, Tadigoppula
European Journal of Organic Chemistry, 2013 , # 29 p. 6491 - 6495
2042-37-7
2-溴苯腈
+
123-54-6
乙酰丙酮
→
反应条件
73013-48-6
(2-氰基苯基)乙酮
反应条件
potassium tert-butylate; ammonium chloride in ammonia 3 h; Irradiation;
参考文献
Beugelmans, R.; Bois-Choussy, M.; Boudet, B.
Tetrahedron, 1982 , vol. 38, # 23 p. 3479 - 3483
201230-82-2
+
2042-37-7
2-溴苯腈
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
746652-00-6
2-(2-甲氧基苯甲酰基)苯甲腈
反应条件
N,N,N',N,-tetramethylethylenediamine; α-n-hexadecene; palladium diacetate; di-(1-adamantyl)-n-butylphosphine in toluene T=100°C; Suzuki reaction; P=3750.38 Torr; 24 h; AutoclaveInert atmosphere;
参考文献
Neumann, Helfried; Brennfuehrer, Anne; Beller, Matthias
Chemistry - A European Journal, 2008 , vol. 14, # 12 p. 3645 - 3652
2042-37-7
2-溴苯腈
+
292638-85-8
丙烯酸甲酯
→
反应条件
18454-44-9
反应条件
tetrabutyl-ammonium chloride; sodium hydrogencarbonate; palladium diacetate in N,N-dimethyl-formamide T=90°C; 24 h;
参考文献
Busacca, Carl A.; Johnson, Robert E.
Tetrahedron Letters, 1992 , vol. 33, # 2 p. 165 - 168
2042-37-7
2-溴苯腈
→
反应条件
66192-31-2
反应条件
1: 97 percent / NaHCO3, (n-Bu)4NCl / Pd(OAc)2 / dimethylformamide / 24 h / 90 °C 2: 67 percent / TEA / Pd(OAc)2 / acetonitrile / 48 h / 100 °C 3: 75 percent / H2 / 10percent Pd/C, PtO2 / ethanol; various solvent(s) / 1) 50 deg C. vent, 2) 68 deg C, 2 h View Scheme
参考文献
Busacca, Carl A.; Johnson, Robert E.
Tetrahedron Letters, 1992 , vol. 33, # 2 p. 165 - 168
2042-37-7
2-溴苯腈
+
13922-41-3
→
反应条件
66252-14-0
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in ethanol; water; toluene T=80°C; Suzuki-Miyaura cross coupling reaction; Inert atmosphere;
参考文献
Tnay, Ya Lin; Chen, Cheng; Chua, Yi Yuan; Zhang, Line; Chiba, Shunsuke
Organic Letters, 2012 , vol. 14, # 13 p. 3550 - 3553
90-14-2
+
2042-37-7
2-溴苯腈
→
反应条件
604-53-5
+
66252-14-0
反应条件
tetrabutylammomium bromide; N-ethyl-N,N-diisopropylamine; palladium diacetate in xylene T=130°C; 42 h;
参考文献
Hassan, Jwanro; Hathroubi, Chokri; Gozzi, Christel; Lemaire, Marc
Tetrahedron, 2001 , vol. 57, # 37 p. 7845 - 7855
104-92-7
+
2042-37-7
2-溴苯腈
→
反应条件
82303-13-7
+
131379-17-4
反应条件
trifluoroacetic acid; cobalt(II) dibromide; zinc dibromide; zinc in 1.4-dicyano 1-butene; acetonitrile Conversion of starting material;
参考文献
Perichon, Jacques; Gosmini, Corinne; Fillon, Hyacinthe
Patent: US2004/236155 A1, 2004 ;
Location in patent: Page 5; 6 ;
75-77-4
+
2042-37-7
2-溴苯腈
→
反应条件
86863-90-3
反应条件
1: 2-cyanophenyl bromide With n-butyllithium in tetrahydrofuran; hexane T=20°C; 2: chloro-trimethyl-silane in tetrahydrofuran; hexane T=20°C;
参考文献
Nagaki, Aiichiro; Kim, Heejin; Usutani, Hirotsugu; Matsuo, Chika; Yoshida, Jun-Ichi
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 5 p. 1212 - 1217
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