1,2-二(苯基)丙-1-酮合成路线 (共 138 条)
反应条件
in tetrahydrofuran
T=-40 - 20°C; 0.2 h;
参考文献
Ooi, Takashi; Goto, Ryoji; Maruoka, Keiji
Journal of the American Chemical Society, 2003 , vol. 125, # 35 p. 10494 - 10495
反应条件
tris(trifluoroacetoxy)-λ3-iodane in tetrachloromethane
T=23°C; 3 h;
参考文献
Futami; Nishino; Kurosawa
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 10 p. 3182 - 3186
反应条件
water; oxygen; copper diacetate in dichloromethane
T=80°C; 16 h; Reagent/catalystTemperatureConcentration; regioselective reaction;
参考文献
Xu, Ze-Feng; Cai, Chen-Xin; Liu, Jin-Tao
Organic Letters, 2013 , vol. 15, # 9 p. 2096 - 2099
反应条件
ethanol; sodium ethanolate
anschliessend Behandeln mit Methyljodid, zuletzt bei Siedetemperatur;
参考文献
Kayser
Annales de Chimie (Cachan, France), 1936 , vol. <11> 6, p. 145,176
Full Text Show Details
Bruzau
Annales de Chimie (Cachan, France), 1934 , vol. <11> 1, p. 257,276
反应条件
water; oxygen; copper diacetate in dichloromethane
T=80°C; 16 h; regioselective reaction;
参考文献
Xu, Ze-Feng; Cai, Chen-Xin; Liu, Jin-Tao
Organic Letters, 2013 , vol. 15, # 9 p. 2096 - 2099
反应条件
nickel in ethylene glycol dimethyl ether
T=85°C; 0.25 h;
参考文献
Inaba, Shin-ichi; Rieke, Reuben D.
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1373 - 1381
反应条件
sodium hexamethyldisilazane in tetrahydrofuran
T=-78°C; 96 h;
参考文献
Simonyiova, Sona; Wanner, Klaus T.
Tetrahedron, 2008 , vol. 64, # 22 p. 5107 - 5110
反应条件
Et2AlSPh in hexane
T=25°C; 0.2 h; Title compound not separated from byproducts;
参考文献
Kanemoto, Shigekazu; Morizawa, Yoshitomi; Oshima, Koichiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 12 p. 3941 - 3942
反应条件
2,3,5,6-tetramethylpyrazine N,N'-dioxide; [RuCl(C60H44N2O2)(NO)] in 1,4-dioxane
T=20°C; 17.5 h; Irradiation; Title compound not separated from byproducts;
参考文献
Nakata, Kenya; Takeda, Tsuyoshi; Mihara, Jun; Hamada, Tetsuya; Irie, Ryo; Katsuki, Tsutomu
Chemistry - A European Journal, 2001 , vol. 7, # 17 p. 3776 - 3782
反应条件
palladium diacetate in tetrahydrofuran; chlorobenzene
参考文献
Yale University
Patent: US6072073 A1, 2000 ;