2,6-双[1-(2,6-二异丙苯亚氨基)乙基]吡啶合成路线 （共 4 条）
反应条件
toluene-4-sulfonic acid in methanol Reflux;
参考文献
MOMENTIVE PERFORMANCE MATERIALS INC.; CORNELL UNIVERSITY
Patent: WO2011/6044 A2, 2011 ;
Location in patent: Page/Page column 22-23 ;
反应条件
formic acid in methanol Reflux;
参考文献
Wang, Xin; Yang, Yulin; Fan, Ruiqing; Jiang, Zhaohua
New Journal of Chemistry, 2010 , vol. 34, # 11 p. 2599 - 2604
反应条件
1.1: sodium ethanolate / ethyl acetate / 20 h / Reflux 1.2: 20 h / 0 °C / Reflux 2.1: toluene-4-sulfonic acid / methanol / Reflux View Scheme
参考文献
MOMENTIVE PERFORMANCE MATERIALS INC.; CORNELL UNIVERSITY
Patent: WO2011/6044 A2, 2011 ;
反应条件
in tetrahydrofuran under Ar; Ti complex treated with THF; refluxed for 2 h; solvent removed in vac.; detd. by IR and (1)H NMR spectra;
参考文献
Calderazzo, Fausto; Englert, Ulli; Pampaloni, Guido; Santi, Roberto; Sommazzi, Anna; Zinna, Marianna
Dalton Transactions, 2005 , # 5 p. 914 - 922
