反应条件
1: sodium azide; ammonium chloride / methanol / 6.5 h / 10 - 20 °C 2: toluene / 1 h / 20 °C 3: toluene / 7 h / |Reflux 4: boron trifluoride diethyl etherate / 17 h / 0 - 20 °C 5: sulfuric acid / ethanol / 16 h / 78 °C 6: sodium carbonate / 0.5 h / 20 °C / pH 6.5 - 7 7: sodium azide / water; ethanol / 24 h / |Reflux 8: triphenylphosphine; acetic acid / water; tetrahydrofuran / 16 h / 45 °C 9: phosphoric acid / water; ethyl acetate; ethanol / 50 - 55 °C View Scheme
参考文献
Russian Chemical Bulletin, , vol. 62, # 1 p. 163 - 170
Izv. Akad. Nauk, Ser. Khim., , vol. 62, # 1 p. 165 - 171,7
