1H,1H,2H,2H-全氟己-1-醇合成路线 （共 16 条）
反应条件
triethylamine in tetrahydrofuran T=0°C; 2 h;
参考文献
EP1452161 A1, ;
Page/Page column 8 ;
反应条件
triethylamine; benzenesulfonyl chloride; Sumilizer GM in dichloromethane T=20 - 40°C; 1 h;
参考文献
TOKUYAMA CORPORATION; DAIKIN INDUSTRIES, LTD.
Patent: US2009/23948 A1, 2009 ;
Location in patent: Page/Page column 5 ;
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane; 1,2,2-trifluoro-trichloroethane T=30°C; 18 h;
参考文献
Krupers, Maarten J.; Moeller, Martin
Journal of Fluorine Chemistry, 1997 , vol. 82, # 2 p. 119 - 124
反应条件
air; chlorine T=22.85°C; P=750 Torr; UV-irradiation; Product distribution;
参考文献
Ellis, David A.; Martin, Jonathan W.; De Silva, Amila O.; Mabury, Scott A.; Hurley, Michael D.; Sulbaek Andersen, Mads P.; Wallington, Timothy J.
Environmental Science and Technology, 2004 , vol. 38, # 12 p. 3316 - 3321
反应条件
1: 3,3,4,4,5,5,6,6,6-nonafluorohexan-1-ol With sodium hydroxide T=20°C; 1 h; 2: 1-(Chloromethyl)-4-vinylbenzene With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane T=40°C; 15 h;
参考文献
Andruzzi, Luisa; Chiellini, Emo; Galli, Giancarlo; Li, Xuefa; Kang, Seok H.; Ober, Christopher K.
Journal of Materials Chemistry, 2002 , vol. 12, # 6 p. 1684 - 1692
反应条件
1: 98 percent / CrO3, H2SO4 / acetone; diethyl ether / 0.08 h
2: 80 percent / PCl5 / diethyl ether / 2 h / Heating
View Scheme
参考文献
Achilefu, Samuel; Mansuy, Laurence; Selve, Claude; Thiebaut, Sylvie
Journal of Fluorine Chemistry, 1995 , vol. 70, # 1 p. 19 - 26
