1-碘-1H,1H,2H,2H-全氟辛烷 合成路线 （共 102 条）
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
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反应条件
反应条件
phosphoric acid; phosphorus pentoxide; potassium iodide T=120°C; 4 h;
参考文献
Peroche, Sandrine; Parrot-Lopez, Helene
反应条件
disodium hydrogenphosphate; sodium dithionite in acetonitrile T=40 - 45°C; 3 h;
参考文献
Qing, Feng-Ling; Ji, Min; Lu, Ronghua; Yan, Kelu; Mao, Zhiping
反应条件
copper; zinc; 1,1-dibromomethane in dimethyl sulfoxide T=20°C;
参考文献
Journal of Fluorine Chemistry, , vol. 20, p. 255 - 266
反应条件
manganese in N,N-dimethyl-formamide T=60°C;
参考文献
Werner, Konrad Von
反应条件
copper; zinc in dimethyl sulfoxide T=20°C;
参考文献
Journal of Fluorine Chemistry, , vol. 20, p. 255 - 266
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反应条件
2043-53-0 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷 +
参考文献
EP1757578 A1, ;
反应条件
magnesium 1) Et2O, reflux, 3 h; 2) Et2O, RT, 15 h; Yield given. Multistep reaction;
参考文献
Moreau,P.; Naji,N.
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反应条件
324063-66-3 双(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)氧化锡
反应条件
1: Mg / tetrahydrofuran; diethyl ether 2: tetrachloromethane 3: NaOH / water; tetrahydrofuran View Scheme
参考文献
Xiang, Jiannan; Orita, Akihiro; Otera, Junzo
反应条件
1: 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodooctane With chloro-trimethyl-silane; ethylene dibromide; zinc in tetrahydrofuran T=25°C; 12 h; 2: 4-bromo-1-iodobenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=45°C; 24 h; Further stages.;
参考文献
Zhang; Luo; Curran
反应条件
[CuCl(cod)]; 4-bromophenylmagnesium bromide in tetrahydrofuran; diethyl ether 1.) -20 deg C to r.t., 2.) r.t., 4 h; Yields of byproduct given;
参考文献
Kainz, Sabine; Luo, Zhiyong; Curran, Dennis P.; Leitner, Walter
