1-碘-1H,1H,2H,2H-全氟辛烷 合成路线 （共 102 条）
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
反应条件
T=140°C; 1 h; var. temp., time, substrate (DMF) investigated; Product distributionRate constant;
参考文献
Brace, Neal O.
反应条件
potassium carbonate in acetonitrile
参考文献
Gibbons, Wayne M.; Rose, Patricia A.; Shannon, Paul J.; Zheng, Hanxing
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反应条件
356055-76-0 4-(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)苄醇
反应条件
1.1: Zn; 1,2-dibromoethane; TMSCl / tetrahydrofuran / 15 h / 20 °C 1.2: 48 percent / tetrahydrofuran / 12 h / 45 °C 2.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -40 °C 3.1: 0.366 g / NaBH4 / ethanol / 16 h / 25 °C View Scheme
参考文献
Curran, Dennis P.; Oderaotoshi, Yoji
2043-53-0 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷 +
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反应条件
反应条件
4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
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反应条件
34451-26-8 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛硫醇
反应条件
1: With thiourea in ethylene glycol dimethyl ether; water 8 h; Heating / reflux; 2: With water; sodium methylate in methanol
参考文献
E. I. DU PONT DE NEMOURS AND COMPNAY
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反应条件
30556-86-6 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛烷胺
反应条件
sodium azide; N2H4*H2O-Raney Ni; hydrazine hydrate Multistep reaction;
参考文献
Ortial, Stephanie; Durand, Gregory; Poeggeler, Burkhard; Polidori, Ange; Pappolla, Miguel A.; Boeker, Jutta; Hardeland, Ruediger; Pucci, Bernard
反应条件
T=160°C; Arbuzov reaction; 16 h;
参考文献
Synthesis, , # 6 art. no. Z21404SS, p. 1012 - 1018
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反应条件
356056-14-9 二异丙基(3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟辛基)硅烷
反应条件
1: 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-iodooctane With tert.-butyl lithium in pentane T=-78 - -15°C; 2: chlorodi(isopropyl)silane in pentane T=-78 - 20°C; Further stages.;
参考文献
Zhang, Qisheng; Rivkin, Alexey; Curran, Dennis P.
2043-53-0 1,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8-十七氟-10-碘庚烷 +
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反应条件
反应条件
4-methoxy-phenol; hydroquinone in tert-butyl alcohol T=180 - 190°C; 6 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
