(4-氰苄基)三苯基氯化膦合成路线 (共 4 条)
反应条件
in benzene 48 h; Reflux;
参考文献
Ho, Jinn-Hsuan; Lee, Ya-Wen; Chen, Ying-Zhe; Chen, Pin-Sian; Liu, Wei-Qi; Ding, Yi-Shun
Tetrahedron, 2013 , vol. 69, # 35 p. 7325 - 7332
反应条件
hydrogenchloride 12 h; Heating; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 21 p. 5643 - 5649
反应条件
1: 18-crown-6 ether; potassium carbonate / dichloromethane / 72 h / 20 °C 2: hydrogenchloride / acetonitrile / 48.5 h / |Irradiation; |Inert atmosphere View Scheme
参考文献
Ho, Jinn-Hsuan; Lee, Ya-Wen; Chen, Ying-Zhe; Chen, Pin-Sian; Liu, Wei-Qi; Ding, Yi-Shun
Tetrahedron, 2013 , vol. 69, # 35 p. 7325 - 7332
反应条件
potassium tert-butylate in methanol Wittig olefination; Heating; Title compound not separated from byproducts;
参考文献
Ashwell, Geoffrey J.; Maxwell, Alison A.; Green, Andrew
Journal of Materials Chemistry, 2002 , vol. 12, # 8 p. 2192 - 2196