4-氯-6-甲氧基吡啶甲酸甲酯合成路线 （共 3 条）
反应条件
1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine / 6 h / 100 °C 2: tert.-butylnitrite; copper dichloride / acetonitrile / 40 - 80 °C View Scheme
参考文献
HEIMANN, Annekatrin; DAHMANN, Georg; GRUNDL, Marc; MUELLER, Stephan Georg; WELLENZOHN, Bernd
Patent: US2013/158042 A1, 2013 ;
反应条件
1: 0.5 h / 150 °C / |Microwave irradiation 2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triethylamine / 6 h / 100 °C 3: tert.-butylnitrite; copper dichloride / acetonitrile / 40 - 80 °C View Scheme
参考文献
HEIMANN, Annekatrin; DAHMANN, Georg; GRUNDL, Marc; MUELLER, Stephan Georg; WELLENZOHN, Bernd
Patent: US2013/158042 A1, 2013 ;
反应条件
water; sodium hydroxide in methanol T=20°C; 12 h;
参考文献
HEIMANN, Annekatrin; DAHMANN, Georg; GRUNDL, Marc; MUELLER, Stephan Georg; WELLENZOHN, Bernd
Patent: US2013/158042 A1, 2013 ;
Location in patent: Paragraph 0482; 0483; 0484; 0485; 0486 ;
