左旋-反式-1,2-环己二胺合成路线 （共 43 条）
参考文献
DABUR RESEARCH FOUNDATION
Patent: US2008/207935 A1, 2008 ;
Location in patent: Page/Page column 7 ;
参考文献
Ng, Neville S.; Leverett, Peter; Hibbs, David E.; Yang, Qianfan; Bulanadi, Jerikho C.; Jie Wu, Ming; Aldrich-Wright, Janice R.
Dalton Transactions, 2013 , vol. 42, # 9 p. 3196 - 3209
反应条件
1: 82 percent / NaOH / H2O / 2 h / 0 °C 2: 92 percent / LiAlH4 / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Arjan, Hitesh; Boyd, Ewan; Coumbarides, Gregory S.; Eames, Jason; Jones, Ray V. H.; Stenson, Rachel A.; Suggate, Michael J.
Tetrahedron Letters, 2005 , vol. 46, # 11 p. 1921 - 1925
反应条件
1: With sodium hydroxide in toluene T=25°C; 2: With lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 14 h;
参考文献
Ma, Meng Lin; Ren, Chuan Hong; Lv, Ya Jing; Chen, Hua; Li, Xian Jun
Chinese Chemical Letters, 2011 , vol. 22, # 2 p. 155 - 158
参考文献
Arjan, Hitesh; Boyd, Ewan; Coumbarides, Gregory S.; Eames, Jason; Jones, Ray V. H.; Stenson, Rachel A.; Suggate, Michael J.
Tetrahedron Letters, 2005 , vol. 46, # 11 p. 1921 - 1925
反应条件
silver(l) oxide in water T=90 - 100°C; 10 - 12 h;
参考文献
US2008/207935 A1, ;
Page/Page column 7 ;
参考文献
Kankyo Kagaku Center Co., Ltd.
Patent: US5395962 A1, 1995 ;
反应条件
in 1,4-dioxane 22 h;
参考文献
Uppadine; Keene; Beer
Journal of the Chemical Society, Dalton Transactions, 2001 , # 14 p. 2188 - 2198
反应条件
triethylamine in 1,4-dioxane; water 4 h; Ambient temperature;
参考文献
Hu, Kejiang; Bradshaw, Jerald S.; Dalley, N.Kent; Krakowiak, Krzysztof E.; Wu, Naijun; Lee,Milton L.
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 2 p. 381 - 388
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane 6 h; Ambient temperature;
参考文献
Trost, Barry M.; Van Vranken, David L.; Bingel, Carsten
Journal of the American Chemical Society, 1992 , vol. 114, # 24 p. 9327 - 9343
