N-甲基-2,4-二硝基苯胺合成路线 (共 102 条)
反应条件
sodium hydroxide; methylamine in water
参考文献
Ciba-Geigy Corporation
Patent: US4138568 A1, 1979 ;
反应条件
in ethanol T=20°C; 15 h;
参考文献
Piersanti, Giovanni; Giorgi, Luca; Bartoccini, Francesca; Tarzia, Giorgio; Minetti, Patrizia; Gallo, Grazia; Giorgi, Fabrizio; Castorina, Massimo; Ghirardi, Orlando; Carminati, Paolo
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 16 p. 2567 - 2571
反应条件
sulfuric acid; nitrogen(IV) oxide in water other oxidant;
参考文献
Bueldt, Andrea; Karst, Uwe
Analytical Chemistry, 1997 , vol. 69, # 17 p. 3617 - 3622
反应条件
water; trifluoroacetic acid in acetonitrile T=80°C; 5 h; Sealed tube;
参考文献
Lee, Sang-Hak; Mu, Yu; Kim, Gun-Woo; Kim, Jin-Seok; Park, Seok-Hwi; Jin, Tian; Lee, Kee-Young; Ham, Won-Hun
Heterocycles, 2013 , vol. 87, # 8 p. 1749 - 1764
反应条件
nitric acid T=-30°C; Nitration; 5 h;
参考文献
Journal of Molecular Structure, , vol. 524, # 1-3 p. 217 - 225
反应条件
bromine; acetic acid T=100°C;
参考文献
Chemische Berichte, , vol. 15, p. 1234
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform 30 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 53, # 9 p. 1887 - 1894
反应条件
hydrogenchloride 12 h; Ambient temperature;
参考文献
Bosch; Salas; Amat; Alvarez; Morgo; Adrover
Tetrahedron, 1991 , vol. 47, # 28 p. 5269 - 5276
反应条件
in dimethyl sulfoxide T=50°C; 2 h;
参考文献
Sekiguchi, Shizen; Ishikura, Hiromi; Hirosawa, Yukitoshi; Ono, Nobuyuki
Tetrahedron, 1990 , vol. 46, # 16 p. 5567 - 5578
反应条件
nitric acid; acetic acid
参考文献
Scientific Proceedings of the Royal Dublin Society, , vol. 17, p. 159,160
Chem.Abstr., , vol. 17, p. 1793