3-苯基-1-对甲苯丙酮合成路线 （共 47 条）
反应条件
indium tribromide in dichloromethane
T=20°C; 0.25 h;
参考文献
Yadav; Reddy; Reddy, M. Sridhar; Parimala
Synthesis, 2003 , # 15 p. 2390 - 2394
反应条件
copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride in acetonitrile
T=60°C; 10 h;
参考文献
Oh, Chang Ho; Reddy, V. Raghava
Tetrahedron Letters, 2004 , vol. 45, # 46 p. 8545 - 8548
反应条件
triethylamine
T=100°C; Sonogashira Cross-Coupling; P=15201 Torr; 24 h; AutoclaveSchlenk technique; chemoselective reaction;
参考文献
Aronica, Laura Antonella; Caporusso, Anna Maria; Tuci, Giulia; Evangelisti, Claudio; Manzoli, Maela; Botavina, Maria; Martra, Gianmario
Applied Catalysis A: General, 2014 , vol. 480, p. 1 - 9
反应条件
copper(l) iodide; C23H30ClN4Pd(1+); triethylamine; triphenylphosphine in benzene
T=60°C; Sonogashira Cross-Coupling; 1 h; Overall yield = 89 percent;
参考文献
Ryabukhin, Dmitry S.; Sorokoumov, Viktor N.; Savicheva, Elizaveta A.; Boyarskiy, Vadim P.; Balova, Irina A.; Vasilyev, Aleksander V.
Tetrahedron Letters, 2013 , vol. 54, # 19 p. 2369 - 2372
反应条件
[{Pd(cinnamyl)Cl}2]; triethylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene
T=110°C; Sonogashira coupling; P=7500.75 Torr; 2 h; Inert atmosphereAutoclave;
参考文献
Wu, Xiao-Feng; Sundararaju, Basker; Neumann, Helfried; Dixneuf, Pierre H.; Beller, Matthias
Chemistry - A European Journal, 2011 , vol. 17, # 1 p. 106 - 110
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl acetamide
T=80°C; P=15200 Torr; 1 h;
参考文献
Kakusawa, Naoki; Kurita, Jyoji
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 5 p. 699 - 702
反应条件
bis-triphenylphosphine-palladium(II) chloride in 1,2-dichloro-ethane
T=80°C; Substitution; 2.5 h;
参考文献
Kakusawa, Naoki; Yamaguchi, Kouichiro; Kurita, Jyoji; Tsuchiya, Takashi
Tetrahedron Letters, 2000 , vol. 41, # 21 p. 4143 - 4146
反应条件
palladium dichloride in acetonitrile
T=20°C; Carbonylation; 6 h;
参考文献
Kang, Suk-Ku; Ryu, Hyung-Chul; Lee, Sang-Woo
Journal of Organometallic Chemistry, 2000 , vol. 610, # 1-2 p. 38 - 41
反应条件
[Pd(PPh3)2(OAc)2] in tetrahydrofuran
20 h;
参考文献
Nozaki, Kyoko; Sato, Naomasa; Takaya, Hidemasa
Journal of Organic Chemistry, 1994 , vol. 59, # 10 p. 2679 - 2681
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; nonafluoro-n-butanesulfonyl fluoride; palladium diacetate; triethylamine in acetonitrile
T=80°C; 16 h; Schlenk techniqueInert atmosphere;
参考文献
Li, Haoquan; Neumann, Helfried; Beller, Matthias; Wu, Xiao-Feng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 12 p. 3183 - 3186
Angew. Chem., 2014 , vol. 126, # 12 p. 3247 - 3250,4
