3-苯基-1-对甲苯丙酮合成路线 (共 47 条)
参考文献
Barat
Journal of the Indian Chemical Society, 1930 , vol. 7, p. 851,859
反应条件
1: 89 percent / ethanol / Heating
2: 75 percent / dilute HCl / methanol / 2 h / 60 - 65 °C
View Scheme
参考文献
Zanina, A. S.; Shergina, S. I.; Sokolov, I. E.; Myasnikova, R. N.
Russian Chemical Bulletin, 1995 , vol. 44, # 4 p. 689 - 694
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1995 , # 4 p. 710 - 714
反应条件
hydroxylamine hydrochloride; sodium acetate in tetrahydrofuran
12 h; Inert atmosphereReflux;
参考文献
Liu, Hai-Ling; Geng, Zhu-Feng; Zhang, Si-Yu; Han, Jie
Heterocycles, 2014 , vol. 89, # 5 p. 1221 - 1227
参考文献
Bishop, Brian C.; Brands, Karel M. J.; Gibb, Andrew D.; Kennedy, Derek J.
Synthesis, 2004 , # 1 p. 43 - 52
反应条件
1: tetra-(n-butyl)ammonium iodide / water / 5 h / |Reflux
2: toluene-4-sulfonic acid / water / 1 h / 20 °C
View Scheme
参考文献
Harigae, Ryo; Moriyama, Katsuhiko; Togo, Hideo
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2049 - 2058
反应条件
1: hydroxylamine hydrochloride; sodium sulfate; pyridine / methanol / 20 °C
2: silver trifluoromethanesulfonate; [(2-benzylpyridyl)AuCl2] / methanol; dichloromethane / 2 h / 20 °C
View Scheme
参考文献
Kung, Karen Ka-Yan; Lo, Vanessa Kar-Yan; Ko, Hok-Ming; Li, Gai-Li; Chan, Pui-Ying; Leung, King-Chi; Zhou, Zhongyuan; Wang, Ming-Zhong; Che, Chi-Ming; Wong, Man-Kin
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 10 p. 2055 - 2070
反应条件
1: With potassium phosphate in dimethyl sulfoxide
T=20°C; 2 h; Schlenk technique;
2: in dimethylsulfoxide-d6
T=140°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Shen, Jinhai; Cheng, Guolin; Cui, Xiuling
Chemical Communications, 2013 , vol. 49, # 90 p. 10641 - 10643