3-(4-甲氧基苯基)-1-苯丙酮合成路线 （共 30 条）
反应条件
1: 24.5 percent / NaN3; AlCl3 / tetrahydrofuran / 156 h / Heating
2: 56 percent / Pb(OAc)4 / tetrahydrofuran / 0.33 h / 6 - 8 °C
View Scheme
参考文献
Fetter; Nagy; Giang; Kajtar-Peredy; Rockenbauer; Korecz; Czira
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 9 p. 1131 - 1139
反应条件
1: 73 percent / NaH / tetrahydrofuran / Heating
2: 24.5 percent / NaN3; AlCl3 / tetrahydrofuran / 156 h / Heating
3: 56 percent / Pb(OAc)4 / tetrahydrofuran / 0.33 h / 6 - 8 °C
View Scheme
参考文献
Fetter; Nagy; Giang; Kajtar-Peredy; Rockenbauer; Korecz; Czira
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 9 p. 1131 - 1139
反应条件
1: caesium carbonate; bis[2-(diphenylphosphino)phenyl] ether; palladium diacetate / dimethyl sulfoxide / 2 h / 100 °C / |Inert atmosphere
2: silica gel; water / dichloromethane / 20 °C / |Inert atmosphere
View Scheme
参考文献
Tang, Ting; Fei, Xiang-Dong; Ge, Zhi-Yuan; Chen, Zhong; Zhu, Yong-Ming; Ji, Shun-Jun
Journal of Organic Chemistry, 2013 , vol. 78, # 7 p. 3170 - 3175
参考文献
Manchot
Justus Liebigs Annalen der Chemie, 1912 , vol. 387, p. 291
反应条件
methanol; hydroxylamine hydrochloride; sodium acetate
参考文献
Tuerck; Behringer
Chemische Berichte, 1965 , vol. 98, p. 3020,3023
参考文献
Weygand; Bauer
Justus Liebigs Annalen der Chemie, 1927 , vol. 459, p. 143
参考文献
Weygand; Bauer
Justus Liebigs Annalen der Chemie, 1927 , vol. 459, p. 143
反应条件
methanol; hydroxylamine hydrochloride
参考文献
Kung, Karen Ka-Yan; Lo, Vanessa Kar-Yan; Ko, Hok-Ming; Li, Gai-Li; Chan, Pui-Ying; Leung, King-Chi; Zhou, Zhongyuan; Wang, Ming-Zhong; Che, Chi-Ming; Wong, Man-Kin
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 10 p. 2055 - 2070
参考文献
Weygand; Bauer
Justus Liebigs Annalen der Chemie, 1927 , vol. 459, p. 143
反应条件
trifluorormethanesulfonic acid
T=-30°C; 0.25 h;
参考文献
Vasilyev, Aleksander V.; Walspurger, Stephane; Pale, Patrick; Sommer, Jean
Tetrahedron Letters, 2004 , vol. 45, # 17 p. 3379 - 3381
