2-苯基-1-丁烯-1-酮合成路线 （共 19 条）
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=120°C; 5 h; Var. aroyl chlorides; Product distribution;
参考文献
Tetrahedron Letters, , vol. 26, # 42 p. 5143 - 5144
反应条件
sodium hydroxide T=25°C; hydration; Kinetics; Further Variations:Solventsconcentration;
参考文献
Andraos; Chiang; Eustace; Kresge; Paine; Popik; Sung
Canadian Journal of Chemistry, 1999 , vol. 77, # 4 p. 459 - 462
反应条件
in hexane; benzene Kinetics; React. of starting materials (C6H6), stirring of soln. (5 h, ambient temp., N2 or Ar) and addn. of hexane after reducing of volume by half in vac.; Pptn. of powder upon standing, removal of solvent and liberated PEt3 by washing, filtn. under N2 and drying in vac.;
参考文献
Galante, Julienne M.; Bruno, Joseph W.; Hazin, Paulette N.; Folting, Kirsten; Huffman, John C.
Organometallics, 1988 , vol. 7, p. 1066 - 1073
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=120°C; 5 h;
参考文献
Mitsudo, Take-aki; Kadokura, Mamoru; Watanabe, Yoshihisa
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3186 - 3192
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=120°C; 5 h;
参考文献
Mitsudo, Take-aki; Kadokura, Mamoru; Watanabe, Yoshihisa
Tetrahedron Letters, 1985 , vol. 26, # 42 p. 5143 - 5144
反应条件
sodium hydride in ethylene glycol dimethyl ether T=20°C; 2.25 h; Irradiation;
参考文献
Fillion, H.; Refouvelet, B.; Pera, M. H.; Dufaud, V.; Luche, J. L.
Synthetic Communications, 1989 , vol. 19, # 19 p. 3343 - 3348
参考文献
Gong, Leyi; Leung-Toung, Regis; Tidwell, Thomas T.
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3634 - 3639
反应条件
lithium diisopropyl amide
1.) THF, -78 gradC 2.) THF, -78 gradC; Yield given. Multistep reaction;
参考文献
Bairgrie, Lynn M.; Leung-Toung, Regis; Tidwell, Thomas T.
Tetrahedron Letters, 1988 , vol. 29, # 14 p. 1673 - 1676
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=120°C; 5 h; reactions with other aroyl chlorides; MechanismProduct distribution;
参考文献
Mitsudo, Take-aki; Kadokura, Mamoru; Watanabe, Yoshihisa
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3186 - 3192
