(1-氨基-3-甲基丁基)磷酸合成路线 (共 11 条)
反应条件
hydrogenchloride 20 h; Heating;
参考文献
Oesapay, George; Szilagyi, Ildiko; Seres, Jenoe
Tetrahedron, 1987 , vol. 43, # 13 p. 2977 - 2984
反应条件
1: 75 percent / 100 °C 2: 12M aq. HCl / 8 h / Heating View Scheme
参考文献
Synthesis, , # 5 p. 370 - 372
反应条件
hydrogenchloride 8 h; Heating; Yield given;
参考文献
Synthesis, , # 5 p. 370 - 372
反应条件
hydrogenchloride 8 h; Heating; Yield given;
参考文献
Synthesis, , # 5 p. 370 - 372
反应条件
hydrogenchloride Yield given;
参考文献
Tetrahedron, , vol. 52, # 32 p. 10685 - 10692
反应条件
2: NaBH(OAc)3 3: aq.HCl View Scheme
参考文献
Tetrahedron, , vol. 52, # 32 p. 10685 - 10692
反应条件
1: 1.) sodium hydrogencarbonate, AgNO3, 2.) bromine / 1.) water, 15 min, in the dark, 2.) CCl4, room temperature, 2 h. 2: 20 percent / NaH / 30 °C 3: 87 percent / cc. hydrochloric acid / 20 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 43, # 13 p. 2977 - 2984
反应条件
hydrogenchloride; acetic acid; phosphorus trichoride 1) 1h, reflux 2) 12h, reflux; Yield given. Multistep reaction;
参考文献
Liebigs Annalen der Chemie, , # 11 p. 1153 - 1155
反应条件
(i) H2, Pd-C, MeOH, (ii) NH3, aq. NaBH4; Multistep reaction;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 28, p. 1949 - 1953
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 28, p. 2118 - 2122
反应条件
(i) H2, Raney-Ni, (ii) aq. HCl, AcOH, (iii) methyloxirane; Multistep reaction;
参考文献
Roczniki Chemii, , vol. 50, p. 477 - 487