1,3-二硫烷-2-甲酸乙酯合成路线 （共 10 条）
反应条件
potassium carbonate; Aliquatreg; 336 in toluene 8 h; Ambient temperature;
参考文献
Lissel, Manfred
Liebigs Annalen der Chemie, 1982 , # 9 p. 1589 - 1601
参考文献
Journal of the Indian Chemical Society, , vol. 5, p. 457
Chem. Zentralbl., , vol. 99, # II p. 2254
参考文献
Journal of the Indian Chemical Society, , vol. 5, p. 546
Chem. Zentralbl., , vol. 99, # II p. 2253
Journal of the Indian Institute of Science, Section A, vol. 11, p. 228
Chem. Zentralbl., , vol. 100, # I p. 1697
参考文献
Journal of the Indian Institute of Science, , vol. <A> 11, p. 227,229
Chem. Zentralbl., , vol. 99, # II p. 2253
反应条件
1: [1,3]dithiolane-2-carboxylic acid ethyl ester With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-78°C; Metallation; 0.916667 h; 2: chloro-trimethyl-silane in tetrahydrofuran; hexane T=-78 - 20°C; silylation;
参考文献
Kiyooka, Syun-Ichi; Hena, Mostofa A.
Journal of Organic Chemistry, 1999 , vol. 64, # 15 p. 5511 - 5523
反应条件
sodium sulfate 1.) hexane, CH2Cl2, 15 h, 2.) hexane, CH2Cl2, RT, 1 h; Yield given. Multistep reaction;
参考文献
Mori, Takehiko; Inokuchi, Hiroo
Chemistry Letters, 1992 , # 9 p. 1873 - 1876
反应条件
sodium sulfate 1.) hexane, CH2Cl2, 15 h, 2.) hexane, CH2Cl2, RT, 1 h; Yield given. Multistep reaction;
参考文献
Mori, Takehiko; Inokuchi, Hiroo
Chemistry Letters, 1992 , # 9 p. 1873 - 1876
反应条件
methanol; sodium tetrahydroborate in diethyl ether
T=20°C; Reduction; 0.25 h;
参考文献
Khanapure, Subhash P.; Saha, Goutam; Sivendran, Sashikala; Powell, William S.; Rokach, Joshua
Tetrahedron Letters, 2000 , vol. 41, # 30 p. 5653 - 5657
反应条件
1: 1.) LDA; / 1.) THF-HMPA-hexane, -78 deg C, 30 min, than -78 to -50 deg C, 1 h; 2.) THF-MHPA-hexane, -78 deg C, than -40 deg C, 1 h
2: 78 percent / p-TsOH / CH2Cl2 / 3 h / Ambient temperature
View Scheme
参考文献
kato, Michiharu; Saito, Hiroaki; Yoshikoshi, Akira
Chemistry Letters, 1984 , p. 213 - 216
反应条件
bis(tri-n-butyltin)oxide in toluene
T=80°C; 10 h;
参考文献
Salomon, Claudio J.; Mata, Ernesto G.; Mascaretti, Oreste A.
Journal of Organic Chemistry, 1994 , vol. 59, # 24 p. 7259 - 7266
