1,2,3,4-四氢环戊[b]吲哚合成路线 (共 42 条)
反应条件
liquid 1-butyl-3-methylimidazolium hydrosulfate T=70°C; Fischer indole synthesis; 3 h;
参考文献
Xu, Dan-Qian; Yang, Wen-Long; Luo, Shu-Ping; Wang, Bing-Tao; Wu, Jian; Xu, Zhen-Yuan
European Journal of Organic Chemistry, 2007 , # 6 p. 1007 - 1012
反应条件
L-(+)-tartaric acid-urea melt T=70°C; Fischer Indole Synthesis; 0.5 h;
参考文献
Gore, Sangram; Baskaran, Sundarababu; Koenig, Burkhard
Organic Letters, 2012 , vol. 14, # 17 p. 4568 - 4571
反应条件
hydrogen; palladium on activated charcoal in methanol 0.75 h;
参考文献
Banwell, Martin G.; Kelly, Brian D.; Kokas, Okanya J.; Lupton, David W.
Organic Letters, 2003 , vol. 5, # 14 p. 2497 - 2500
反应条件
titanium(III) chloride; ammonium acetate in acetone T=20°C; 0.25 h;
参考文献
Iwama, Tetsuo; Birman, Vladimir B.; Kozmin, Sergey A.; Rawal, Viresh H.
Organic Letters, 1999 , vol. 1, # 4 p. 673 - 676
反应条件
sulfuric acid 1 h; Heating;
参考文献
Davis, Paul D.; Neckers, Douglas C.
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 456 - 462
反应条件
dirhodium(II) tetraoctanoate in 1,2-dichloro-ethane T=70°C; 16 h; Inert atmosphereMolecular sieve;
参考文献
Sun, Ke; Liu, Sheng; Bec, Patryk M.; Driver, Tom G.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 7 p. 1702 - 1706
反应条件
FeBr2 in toluene T=140°C; 16 h; Schlenk techniqueInert atmosphere;
参考文献
Nguyen, Quyen; Nguyen, Tuyen; Driver, Tom G.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 620 - 623
反应条件
trifluoroacetic acid in dichloromethane 1.75 h;
参考文献
Wender, Paul A.; White, Alan W.
Tetrahedron, 1983 , vol. 39, # 22 p. 3767 - 3776
反应条件
1: 75 percent / Cu powder / Pd(dba)2 / dimethylsulfoxide / 1 h / 70 °C 2: 90 percent / H2 / 10 percent Pd/C / methanol / 0.75 h View Scheme
参考文献
Organic Letters, , vol. 5, # 14 p. 2497 - 2500
反应条件
caesium carbonate; bis(dibenzylideneacetone)-palladium(0) in toluene T=150°C; 24 h; Inert atmosphere;
参考文献
Tan, Yichen; Hartwig, John F.
Journal of the American Chemical Society, 2010 , vol. 132, # 11 p. 3676 - 3677