2,3-二甲基-2,3-丁二胺合成路线 （共 38 条）
反应条件
1.1: 78 percent / aq. H2SO4 / methanol / 1 h / 20 °C / pH 3 - 4 2.1: m-chloroperbenzoic acid; NaHCO3 / CH2Cl2 / 1 h / Ice cooling 2.2: 12 percent / aq. NaIO4 / CH2Cl2 View Scheme
参考文献
Hirel, Catherine; Vostrikova, Kira E.; Pecaut, Jacques; Ovcharenko, Victor I.; Rey, Paul
Chemistry - A European Journal, 2001 , vol. 7, # 9 p. 2007 - 2014
反应条件
hydrogenchloride; n-butyllithium; acetic acid in tetrahydrofuran; hexane; water
参考文献
Schafer, Bernd; Geneste, Herve
Patent: US2004/92754 A1, 2004 ;
反应条件
in cupric chloride; potassium iodide; nitrogen
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4172838 A1, 1979 ;
Title/Abstract Full Text Show Details
E. I. Du Pont de Nemours and Company
Patent: US4268421 A1, 1981 ;
反应条件
n-butyllithium; ammonium chloride in tetrahydrofuran; methanol; hexane; dichloromethane
参考文献
Bayer Aktiengesellschaft
Patent: US4703119 A1, 1987 ;
反应条件
2: H2 / Raney-Ni View Scheme
参考文献
Kobiro, Kazuya; Nakayama, Atsuyoshi; Hiro, Toshitaka; Suwa, Mitsuhito; Kakiuchi, Kiyomi; et al.
Chemistry Letters, 1990 , # 11 p. 1979 - 1982
反应条件
n-butyllithium in tetrahydrofuran; hexane
反应条件
n-butyllithium; iodine in tetrahydrofuran
参考文献
Ferraris, Dana V.; Li, Jia-He; Kalish, Vincent J.; Zhang, Jie
Patent: US2003/22883 A1, 2003 ;
反应条件
hydrogenchloride; n-butyllithium
参考文献
Takahashi, Tamotsu
Patent: US2003/116755 A1, 2003 ;
反应条件
3,3-dimethyldioxirane
参考文献
Gagnon, Janet L.; Zajac Jr., Walter W.
Tetrahedron Letters, 1995 , vol. 36, # 11 p. 1803 - 1804
反应条件
in diethyl ether ice cooling;
参考文献
Hirel, Catherine; Vostrikova, Kira E.; Pecaut, Jacques; Ovcharenko, Victor I.; Rey, Paul
Chemistry - A European Journal, 2001 , vol. 7, # 9 p. 2007 - 2014
