(E)-A,A’-二氟芪合成路线 （共 24 条）
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
Liu, Qibo; Burton, Donald J.
Organic Letters, 2002 , vol. 4, # 9 p. 1483 - 1485
反应条件
bis(1,5-cyclooctadiene)nickel (0); caesium carbonate; tri-cyclo-hexyl-phosphine in tetrahydrofuran; benzene-d6 T=100°C; 16 h; Inert atmosphere;
参考文献
Daikin Industries; Osaka University; Nagai, Takabumi; Adachi, Kenji; Shibanuma, Takashi; Ogoshi, Sensuke; Ohashi, Masato
Patent: US2013/324757 A1, 2013 ;
Location in patent: Paragraph 0277-0284 ;
反应条件
[Ni0(1,5-cyclooctadiene)2]; triphenylphosphine in tetrahydrofuran; diethyl ether T=20°C; P=2625.26 Torr; 48 h; Product distribution / selectivity;
参考文献
Nagai, Takabumi; Shibanuma, Takashi; Ogoshi, Sensuke; Ohashi, Masato
Patent: US2012/330072 A1, 2012 ;
Location in patent: Page/Page column 7 ;
反应条件
diethyl ether T=-80°C;
参考文献
McGrath; Levine
Journal of the American Chemical Society, 1955 , vol. 77, p. 4168
Full Text View citing articles Show Details
Dixon
Journal of Organic Chemistry, 1956 , vol. 21, p. 400,402
反应条件
pyridine; copper T=100°C; 2 h;
参考文献
Kremlev, M. M.; Maznyi, I. S.; Sereda, S. V.; Yagupol'skii, Yu. L.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 5.1 p. 758 - 761
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 5 p. 982 - 986
参考文献
McGrath; Levine
Journal of the American Chemical Society, 1955 , vol. 77, p. 4168
参考文献
McGrath; Levine
Journal of the American Chemical Society, 1955 , vol. 77, p. 4168
反应条件
zinc(II) chloride; zinc in ethanol; acetic acid; N,N-dimethyl-formamide 10 h; Heating;
参考文献
Ganushchak, N. I.; Bilaya, E. E.; Obushak, N. D.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 2.2 p. 298 - 300
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 2 p. 356 - 359
反应条件
1: 70 percent / CuCl2 / acetone / -15 - 20 °C 2: 21 percent / Zn, ZnCl2 / acetic acid; dimethylformamide; ethanol / 10 h / Heating View Scheme
参考文献
Ganushchak, N. I.; Bilaya, E. E.; Obushak, N. D.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 2.2 p. 298 - 300
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 2 p. 356 - 359
反应条件
1: 70 percent / CuCl2 / acetone / -15 - 20 °C 2: 21 percent / Zn, ZnCl2 / acetic acid; dimethylformamide; ethanol / 10 h / Heating View Scheme
参考文献
Ganushchak, N. I.; Bilaya, E. E.; Obushak, N. D.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 2.2 p. 298 - 300
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 2 p. 356 - 359
