[PdCl(((OC6H4C6H4O)PO)2C6H(tBu)2)]; potassium carbonate in acetonitrile T=40°C; 16 h; Inert atmosphere;
参考文献
Li, Jie; Lutz, Martin; Spek, Anthony L.; Van Klink, Gerard P.M.; Van Koten, Gerard; Klein Gebbink, Robertus J.M.
Journal of Organometallic Chemistry, 2010 , vol. 695, # 24 p. 2618 - 2628
P(C6H5)3 in THF-d8 (tetrahydrofuran-d8) addn. of 3 equiv. of PPh3 and catecholborane to soln. of Rh-complex (25°C, (11)B-NMR monitoring); not isolated;
参考文献
Journal of the American Chemical Society, , vol. 114, # 24 p. 9350 - 9359
P(C6H5)3 in THF-d8 (tetrahydrofuran-d8) addn. of 2 or 3 equiv. of PPh3 to soln. of Rh-complex (25°C, NMR tube, addn. of catecholborane after 40 min), (31)P-NMR monitoring at -80°C; not isolated;
参考文献
Journal of the American Chemical Society, , vol. 114, # 24 p. 9350 - 9359
