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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
辛二酸二乙酯
合成路线
（共 69 条）
109-09-1
2-氯吡啶
+
2969-81-5
4-溴丁酸乙酯
→
反应条件
84199-93-9
+
2050-23-9
辛二酸二乙酯
反应条件
1: ethyl 4-bromobutanoate With nickel(II) bromide trihydrate; bathophenanthroline in N,N-dimethyl-formamide T=40°C; 0.333333 h; 2: alpha-chloropyridine With manganese in N,N-dimethyl-formamide T=40°C; Sealed tube; Reagent/catalystSolventTemperature;
参考文献
Everson, Daniel A.; Buonomo, Joseph A.; Weix, Daniel J.
Synlett, 2014 , vol. 25, # 2 art. no. ST-2013-R0770-L, p. 233 - 238
505-48-6
辛二酸
+
64-17-5
乙醇
→
反应条件
2050-23-9
辛二酸二乙酯
反应条件
sulfuric acid 0.05 h; Microwave irradiation;
参考文献
COUNCIL OF SCIENTIFIC and INDUSTRIAL RESEARCH; Sarma, Jadab Chandra; Bora, Dilip Chandra; Rao, Paruchuri Gangadhar; Ghosh, Balaram; Balwani, Sakshi
Patent: US2013/131350 A1, 2013 ;
Location in patent: Paragraph 0090; 0115-0126 ;
2969-81-5
4-溴丁酸乙酯
+
81167-60-4
4-叔丁基-2-氯-吡啶
→
反应条件
2050-23-9
辛二酸二乙酯
反应条件
1: ethyl 4-bromobutanoate With nickel(II) bromide trihydrate; bathophenanthroline in N,N-dimethyl-formamide T=40°C; 0.333333 h; 2: 4-(tert-butyl)-2-chloropyridine With manganese in N,N-dimethyl-formamide T=40°C; Sealed tube;
参考文献
Everson, Daniel A.; Buonomo, Joseph A.; Weix, Daniel J.
Synlett, 2014 , vol. 25, # 2 art. no. ST-2013-R0770-L, p. 233 - 238
2969-81-5
4-溴丁酸乙酯
+
52334-81-3
2-氯-5-三氟甲基吡啶
→
反应条件
2050-23-9
辛二酸二乙酯
+
1100766-42-4
反应条件
1: ethyl 4-bromobutanoate With nickel(II) bromide trihydrate; sodium iodide in N,N-dimethyl-formamide T=40°C; 0.333333 h; 2: 2-chloro-5-(trifluoromethyl)-pyridine With manganese in N,N-dimethyl-formamide T=40°C; Sealed tube;
参考文献
Everson, Daniel A.; Buonomo, Joseph A.; Weix, Daniel J.
Synlett, 2014 , vol. 25, # 2 art. no. ST-2013-R0770-L, p. 233 - 238
2969-81-5
4-溴丁酸乙酯
→
反应条件
2050-23-9
辛二酸二乙酯
反应条件
manganese; [NiCl2(1,2-dimethoxyethane)]; Ru(4,4′,4''-tri-t-butyl-2,2′;6,2″-terpyridine)Cl3 in N,N-dimethyl-formamide T=40°C; 15.5 h;
参考文献
Prinsell, Michael R.; Everson, Daniel A.; Weix, Daniel J.
Chemical Communications, 2010 , vol. 46, # 31 p. 5743 - 5745
505-48-6
辛二酸
+
64-17-5
乙醇
→
反应条件
14113-01-0
辛二酸氢乙酯
+
2050-23-9
辛二酸二乙酯
反应条件
sulfuric acid in cyclohexane 48 h;
参考文献
Menger, F. M.; Wood, M. G.; Richardson, S.; Zhou, Q.; Elrington, A. R.; Sherrod, M. J.
Journal of the American Chemical Society, 1988 , vol. 110, # 20 p. 6797 - 6803
2969-81-5
4-溴丁酸乙酯
+
183545-05-3
2-氯-5-(三丁基锡烷基)吡啶
→
反应条件
2050-23-9
辛二酸二乙酯
反应条件
1: ethyl 4-bromobutanoate With nickel(II) bromide trihydrate; bathophenanthroline in N,N-dimethyl-formamide T=40°C; 0.333333 h; 2: 2-chloro-5-(tributylstannyl)pyridine With manganese in N,N-dimethyl-formamide T=40°C; Sealed tube;
参考文献
Everson, Daniel A.; Buonomo, Joseph A.; Weix, Daniel J.
Synlett, 2014 , vol. 25, # 2 art. no. ST-2013-R0770-L, p. 233 - 238
109-09-1
2-氯吡啶
+
2969-81-5
4-溴丁酸乙酯
→
反应条件
366-18-7
2,2'-联吡啶
+
84199-93-9
+
2050-23-9
辛二酸二乙酯
反应条件
1: ethyl 4-bromobutanoate With bathophenanthroline; niobium bromide in N,N-dimethyl-formamide T=40°C; 0.333333 h; 2: alpha-chloropyridine With manganese in N,N-dimethyl-formamide T=40°C; Sealed tube; Overall yield = 34 percentChromat.;
参考文献
Synlett, , vol. 25, # 2 art. no. ST-2013-R0770-L, p. 233 - 238
109-09-1
2-氯吡啶
+
2969-81-5
4-溴丁酸乙酯
→
反应条件
110-86-1
吡啶
+
84199-93-9
+
2050-23-9
辛二酸二乙酯
反应条件
1: ethyl 4-bromobutanoate With nickel(II) bromide trihydrate; Ru(4,4′,4''-tri-t-butyl-2,2′;6,2″-terpyridine)Cl3 in N,N-dimethyl-formamide T=40°C; 0.333333 h; 2: alpha-chloropyridine With manganese in N,N-dimethyl-formamide T=40°C; Sealed tube; Overall yield = 15 percentChromat.;
参考文献
Synlett, , vol. 25, # 2 art. no. ST-2013-R0770-L, p. 233 - 238
591-50-4
碘苯
+
2969-81-5
4-溴丁酸乙酯
→
反应条件
92-52-4
联苯
+
2050-23-9
辛二酸二乙酯
+
10031-93-3
4-苯丁酸乙酯
反应条件
pyridine; N,N'-dimethyl-N,N'-propyleneurea; manganese; H7I2NiO3.5; bis(1,2-diphenylphosphino)benzene; 4,4'-di-tert-butyl-2,2'-dipyridyl T=80°C; 7 h; Inert atmosphere;
参考文献
Everson, Daniel A.; Shrestha, Ruja; Weix, Daniel J.
Journal of the American Chemical Society, 2010 , vol. 132, # 3 p. 920 - 921
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