(2,5-二羟基苯基)-苯基甲酮合成路线 （共 18 条）
反应条件
in benzene
Friedel-Crafts acylation; 30 h; Inert atmosphereSolar irradiationSealed vessel;
参考文献
Arenas, Paola; Pena, Andres; Rios, David; Benites, Julio; Muccioli, Giulio G.; Calderon, Pedro Buc; Valderrama, Jaime A.
Molecules, 2013 , vol. 18, # 8 p. 9818 - 9832
反应条件
(NH4)2S2O8; silver nitrate in water; acetonitrile
T=70°C; 2 h;
参考文献
Kraus, George A.; Melekhov, Alex
Tetrahedron Letters, 1998 , vol. 39, # 23 p. 3957 - 3960
反应条件
aluminum oxide; methanesulfonic acid
T=140°C; 1 h;
参考文献
Sharghi, Hashem; Kaboudin, Babak
Journal of Chemical Research, Miniprint, 1998 , # 10 p. 2678 - 2695
反应条件
zinc
T=49 - 51°C; Friedel-Crafts acylation; 0.00972222 h; microwave irradiation;
参考文献
Paul, Satya; Nanda, Puja; Gupta, Rajive; Loupy, Andre
Synthesis, 2003 , # 18 p. 2877 - 2881
反应条件
1: n-BuLi / diethyl ether / Ambient temperature
2: manganese dioxide
3: aluminum triiodide, tetrabutylammonium iodide
View Scheme
参考文献
Cassis, Raul; Fernandez, Monica; Tapia, Ricardo; Valderrama, Jaime A.
Synthetic Communications, 1987 , vol. 17, # 9 p. 1077 - 1088
反应条件
boron trifluoride diethyl etherate in benzene
crossover Friess rearrangement; 3 h; Heating;
参考文献
Khanna, R. N.; Singh, K. P.; Sharma, Jyotsana
Organic Preparations and Procedures International, 1992 , vol. 24, # 6 p. 687 - 690
反应条件
1: AlCl3; carbon disulfide / und Erwaermen des nach der Hydrolyse erhaltenen Reaktionsprodukts mit AlCl3 in Benzol
2: aqueous HI; acetic acid; acetic acid anhydride
View Scheme
参考文献
Bogert; Howells
Journal of the American Chemical Society, 1930 , vol. 52, p. 837,844
反应条件
hydrogen iodide; acetic anhydride; acetic acid
参考文献
Bogert; Howells
Journal of the American Chemical Society, 1930 , vol. 52, p. 837,844
反应条件
boron trifluoride diethyl etherate in benzene
cross Fries reaction; 0.5 h; microwave irradiation;
参考文献
Thapliyal; Aggarwal
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 9 p. 706 - 708
反应条件
boron trifluoride diethyl etherate in benzene
cross Fries reaction; 0.5 h; microwave irradiation;
参考文献
Thapliyal; Aggarwal
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 9 p. 706 - 708
