1-Azabicyclo[2.2.2]octan-3-one; copper diacetate; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in toluene T=20°C; Heck reaction; 48 h; Title compound not separated from byproducts;
参考文献
Advanced Synthesis and Catalysis, , vol. 347, # 1 p. 185 - 195
1: 1-bromocyclohexane With [Fe(C2H4)4][Li(tmeda)]2 in tetrahydrofuran 2: 4-chlorophenyl magnesium halide in tetrahydrofuran; diethyl ether T=0°C; Further stages.;
参考文献
Journal of the American Chemical Society, , vol. 130, # 27 p. 8773 - 8787
1: 4-ClC6H4MgX With indium(III) chloride in tetrahydrofuran T=20°C; 1 h; 2: 6-acetoxy-1-cyclohexene-1-carbonitrile With triphenylphosphine; tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran Heating;
参考文献
Journal of Organic Chemistry, , vol. 69, # 11 p. 3957 - 3960
