diisobutylaluminium hydride in tetrahydrofuran T=-78 - 67°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yuan, Kaixu; Scott, William J.
Journal of Organic Chemistry, 1990 , vol. 55, # 25 p. 6188 - 6194
1: 2 h / 20 °C 2: trifluoroacetic acid / 6 h / 20 °C 3: (CO2H)2 / H2O; diethyl ether / 14 h View Scheme
参考文献
Adlington, Robert M.; Baldwin, Jack E.; Bottaro, Jeffrey C.; Perry, Matthew W. D.
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 1040 - 1041
Baldwin, Jack E.; Adlington, Robert M.; Bottaro, Jeffrey C.; Kolhe, Jayant N.; Perry, Matthew W. D.; Jain, Ashok U.
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Baldwin, Jack E.; Bottaro, Jeffrey C.; Kolhe, Jayant N.; Adlington, Robert M.
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