二(3-甲基丁基)碳酸酯合成路线 （共 24 条）
反应条件
dibutyl-bis(3-methylbutyloxy)tin; 1,1,3,3-tetrabutyl-1,3-bis(3-methylbutyloxy)distannoxane T=120°C; 4 h; AutoclaveIndustry scale; Product distribution / selectivity;
参考文献
Shinohata, Masaaki; Miyake, Nobuhisa
Patent: US2010/292496 A1, 2010 ;
Location in patent: Page/Page column 46 ;
反应条件
1,1,3,3-tetrabutyl-1,3-bis(3-methylbutyloxy)distannoxane T=120°C; P=30003 Torr; 4 h; Industry scaleAutoclave;
参考文献
Asahi Kasei Chemicals Corporation
Patent: EP2275406 A1, 2011 ;
Location in patent: Page/Page column 39-40 ;
反应条件
T=120°C; P=30003 Torr; Autoclave;
参考文献
Shinohata, Masaaki; Miyake, Nobuhisa
Patent: US2010/292496 A1, 2010 ;
Location in patent: Page/Page column 56 ;
反应条件
T=60 - 120°C; P=4125.41 - 30753.1 Torr; 6 h; Large scale; ConcentrationTemperaturePressure;
参考文献
Asahi Kasei Chemicals Corporation; Miyake, Nobuhisa; Onishi, Kazuhiro; Tomoyasu, Kazuo; Bijanto, Budianto
Patent: US8362289 B2, 2013 ;
Location in patent: Page/Page column 79; 80; 81 ;
反应条件
T=120°C; 4 h; Industry scaleAutoclave;
参考文献
Asahi Kasei Chemicals Corporation
Patent: EP2226328 A1, 2010 ;
Location in patent: Page/Page column 75 ;
反应条件
1,1,3,3-tetrabutyl-1,3-bis(3-methylbutyloxy)distannoxane T=120°C; P=30003 Torr; Product distribution / selectivity;
参考文献
Asahi Kasei Chemicals Corporation
Patent: EP2078724 A1, 2009 ;
Location in patent: Page/Page column 33 ;
反应条件
1,1,3,3-tetraoctyl-1,3-bis(3-methylbutyloxy)distannoxane T=120°C; P=30003 Torr; Product distribution / selectivity;
参考文献
Asahi Kasei Chemicals Corporation
Patent: EP2078724 A1, 2009 ;
Location in patent: Page/Page column 38-39 ;
反应条件
T=120°C; P=30003 - 37503.8 Torr; 2.16667 h; Product distribution / selectivity;
参考文献
Asahi Kasei Chemicals Corporation
Patent: EP1535896 A1, 2005 ;
Location in patent: Page/Page column 33 ;
反应条件
T=120°C; P=30003 - 37503.8 Torr; 4.16667 h; Product distribution / selectivity;
参考文献
Asahi Kasei Chemicals Corporation; Miyake, Nobuhisa; Onishi, Kazuhiro; Tomoyasu, Kazuo; Bijanto, Budianto
Patent: US8362289 B2, 2013 ;
Location in patent: Page/Page column 73; 74; 75 ;
反应条件
1: 3-methyl-1-butanol; carbon dioxide; dioctyl-bis(3-methylbutyloxy)tin With 1,1,3,3-tetraoctyl-1,3-bis(3-methylbutyloxy)distannoxane T=120°C; P=30003 Torr; 2: acetic anhydride T=25°C; 1 h; Inert atmosphere; Product distribution / selectivity;
参考文献
Asahi Kasei Chemicals Corporation
Patent: EP2078724 A1, 2009 ;
Location in patent: Page/Page column 38-39 ;
