6-氯-2H-色烯-2-酮合成路线 (共 22 条)
参考文献
Baesecke
Justus Liebigs Annalen der Chemie, 1870 , vol. 154, p. 85
反应条件
boron tribromide in toluene
T=110°C; 4 h; Inert atmosphere;
参考文献
Teichert, Johannes F.; Feringa, Ben L.
Chemical Communications, 2011 , vol. 47, # 9 p. 2679 - 2681
反应条件
1: ethyl ethynyl ether With n-butyllithium in tetrahydrofuran; hexane
T=-78 - 0°C; 4.33333 h; Inert atmosphere;
2: 5-chloro-2-hydroxybenzaldehyde in tetrahydrofuran; hexane
T=-78 - 20°C; 2 h; Inert atmosphere;
参考文献
Sridhar Reddy, Maddi; Thirupathi, Nuligonda; Babu, Madala Hari
European Journal of Organic Chemistry, 2012 , # 29 p. 5803 - 5809
反应条件
triethylamine; benzylamine in chloroform
T=55°C; 3 h;
参考文献
Wei, Jia; Wang, Pengcheng; Jia, Qianfa; Huang, Jiaoyao; Du, Zhiyun; Zhang, Kun; Wang, Jian
European Journal of Organic Chemistry, 2013 , # 21 p. 4499 - 4502
反应条件
4-(N,N-dimethlyamino)pyridine; 4-mesityl-3-(4-methoxyphenyl)-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate in ethyl acetate
T=80°C; 15 h; Inert atmosphere;
参考文献
Zeitler, Kirsten; Rose, Christopher A.
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1759 - 1762
反应条件
1: toluene / Heating
2: 60 percent / BBr3 / toluene / 3 h / Heating
View Scheme
参考文献
Dubuffet; Loutz; Lavielle
Synthetic Communications, 1999 , vol. 29, # 6 p. 929 - 936
反应条件
boron tribromide in toluene
3 h; Heating;
参考文献
Dubuffet; Loutz; Lavielle
Synthetic Communications, 1999 , vol. 29, # 6 p. 929 - 936
反应条件
copper in quinoline
0.166667 h; Heating;
参考文献
Oda, Noriichi; Yoshida, Yukio; Nagai, Shin-ichi; Ueda, Taisei; Sakakibara, Jinsaku
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 5 p. 1796 - 1802
反应条件
T=750°C; P=0.005 Torr; 0.0833333 h;
参考文献
Cartwright, Gary A.; McNab, Hamish
Journal of Chemical Research - Part S, 1997 , # 8 p. 296 - 297
反应条件
acetic acid
6 h; Heating;
参考文献
Harvey; Cortez; Ananthanarayan; Schmolka
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 3936 - 3943