反应条件
1: 98 percent / toluene / Heating 2: 95 percent / LiAlH4, AlCl3 / tetrahydrofuran / a) -78 deg C, 45 min, b) -78 deg C to r.t., 20 min, c) r.t., 15 min 3: 90 percent / triethylphosphine / pyridine / 14 h / Heating 4: 51 percent / lithium di-tert-butylbiphenylide / tetrahydrofuran / a) -78 deg C, 1 h, b) 0 deg C, 50 min View Scheme
参考文献
Amat, Mercedes; Arroniz, Carlos; Molins, Elies; Escolano, Carmen; Bosch, Joan
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 7 p. 2175 - 2184
