1-(对甲苯基)-1H-吡唑合成路线 (共 10 条)
反应条件
copper (II) acetate monohydrate; caesium carbonate in N,N-dimethyl-formamide T=110°C; 24 h; Inert atmosphere;
参考文献
Xu, Zhong-Lin; Li, Hong-Xi; Ren, Zhi-Gang; Du, Wei-Yuan; Xu, Wei-Chang; Lang, Jian-Ping
Tetrahedron, 2011 , vol. 67, # 29 p. 5282 - 5288
反应条件
o-hydroxybenzaldehyde oxime; caesium carbonate; copper(I) oxide in acetonitrile T=82°C; 36 h;
参考文献
Cristau, Henri-Jean; Cellier, Pascal P.; Spindler, Jean-Francis; Taillefer, Marc
European Journal of Organic Chemistry, 2004 , # 4 p. 695 - 709
反应条件
[Cu30I16(5-methyl-4-(p-tolyl)pyrimidine-2-thiolato)12(μ10-S4)] in methanol 5 h; Reflux; TemperatureReagent/catalyst;
参考文献
Li, Hong-Xi; Zhao, Wei; Li, Hai-Yan; Xu, Zhong-Lin; Wang, Wen-Xia; Lang, Jian-Ping
Chemical Communications, 2013 , vol. 49, # 39 p. 4259 - 4261
反应条件
copper diacetate in dichloromethane; N,N-dimethyl-formamide T=90°C; 4 h; other substrates;
参考文献
Lopez-Alvarado, Pilar; Avendano, Carmen; Menendez, J. Carlos
Tetrahedron Letters, 1992 , vol. 33, # 5 p. 659 - 662
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Lopez-Alvarado, Pilar; Avendano, Carmen; Menendez, J. Carlos
Journal of Organic Chemistry, 1995 , vol. 60, # 17 p. 5678 - 5682
反应条件
O-(p-toluenesulfonyl)-hydroxylamine in dichloromethane T=20°C; 24 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 21 p. 2773 - 2782
反应条件
potassium hydroxide in dimethyl sulfoxide T=120°C; 48 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 76, # 2 p. 654 - 660
反应条件
in dichloromethane T=20°C; 24 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 21 p. 2773 - 2782
反应条件
hydrogenchloride in ethanol; water Heating;
参考文献
Magnetic Resonance in Chemistry, , vol. 49, # 8 p. 537 - 542
反应条件
T=600°C; P=0.001 - 0.005 Torr; 0.666667 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1569 - 1572
反应条件
trifluoroacetic acid Duff Aldehyde Synthesis; 12 h; Reflux; chemoselective reaction;
参考文献
De Oliveira; Mairink; Pazini; Liao; Viegas Jr.; Cunha; Oliveira; Paz Jr.; Eberlin; Menegatti, Ricardo
Synthetic Communications, 2013 , vol. 43, # 12 p. 1633 - 1639