2-氯-3-碘-6-(三氟甲基)吡啶合成路线 (共 2 条)
反应条件
n-butyllithium; iodine; diisopropylamine in tetrahydrofuran; hexane 1.) -85 deg C, 4 h;
参考文献
Mongin, Florence; Tognini, Antonio; Cottet, Fabrice; Schlosser, Manfred
Tetrahedron Letters, 1998 , vol. 39, # 13 p. 1749 - 1752
反应条件
1: With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-75°C; 0.75 h; 2: With hydrogenchloride in tetrahydrofuran; hexane T=25°C; Further stages.;
参考文献
European Journal of Organic Chemistry, , # 18 p. 3793 - 3798