[3-(氨基甲基)苯基]氨基甲酸叔丁酯合成路线 （共 4 条）
反应条件
Si-dimethylamine in N,N-dimethyl-formamide 1 h;
参考文献
WO2008/86047 A1, ;
Page/Page column 83-84 ;
WO 2008/086047 A1
反应条件
acetic acid in 1,4-dioxane; water T=20°C; pH=4.5; regioselective reaction;
参考文献
Synthesis, , # 2 p. 283 - 289
反应条件
1: isobutyl chloroformate / dichloromethane / 0.25 h 2: hydrogenchloride / water / 1 h 3: sodium azide; tetrabutylammomium bromide / acetone / 0.5 h 4: triphenylphosphine / tetrahydrofuran; water / 5 h View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 16 p. 4879 - 4883
反应条件
1: hydrogenchloride / water / 1 h 2: sodium azide; tetrabutylammomium bromide / acetone / 0.5 h 3: triphenylphosphine / tetrahydrofuran; water / 5 h View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 16 p. 4879 - 4883
