N-(5-氨基-1-羧基戊基)亚胺二乙酸三-t-丁酯合成路线 (共 2 条)
反应条件
dimercaptoethane; tri-iso-propylsilane; phenol; trifluoroacetic acid T=20°C; 4 h;
参考文献
Lata, Suman; Gavutis, Martynas; Tampe, Robert; Piehler, Jacob
Journal of the American Chemical Society, 2006 , vol. 128, # 7 p. 2365 - 2372
反应条件
Multi-step reaction with 2 steps 1: 85 percent / EDIPA / dimethylformamide / 12 h / 55 °C2: 94 percent / H2 / Pd/C / methanol / 6 h / 20 °C
参考文献
Lata, Suman; Gavutis, Martynas; Tampe, Robert; Piehler, Jacob Journal of the American Chemical Society, 2006 , vol. 128, # 7 p. 2365 - 2372