7-甲氧基吲哚-2-甲酸乙酯合成路线 (共 13 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol T=20°C; 24 h;
参考文献
US2009/238761 A1, ;
Page/Page column 26 ;
US 20090238761 A1
反应条件
1: in toluene T=20°C; Wittig reaction; 2: With triphenylphosphine; [MoO2Cl2(dmf)2] in toluene 24 h; Heating; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 4-5 p. 713 - 718
反应条件
aluminium trichloride in various solvent(s) T=0°C; 0.25 h;
参考文献
Synthesis, , vol. NO. 9, p. 738 - 740
反应条件
copper(l) iodide in dimethyl sulfoxide T=50°C; 0.166667 h; Ionic liquidInert atmosphereMicrowave irradiationSealed tube;
参考文献
Journal of the Brazilian Chemical Society, , vol. 22, # 11 p. 2036 - 2039
反应条件
potassium ethanolate in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; diethyl ether; ethanol
参考文献
US6169107 A, ;
US 6169107 B1
反应条件
in diethyl ether Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 44, # 1 p. 55 - 61
反应条件
hydrogen; platinum(IV) oxide in ethanol T=20°C; Reduction; Cyclization; Reissert indole synthesis; Product distribution; Further Variations:CatalystsSolvents;
参考文献
Synlett, , # 8 p. 1196 - 1198
反应条件
1: sodium ethanolate / ethanol / -10 - 0 °C / Inert atmosphere 2: hexane / 0.08 h / 200 °C / 9000.9 - 9750.98 Torr / Microwave irradiation; Inert atmosphere View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 19, # 4 p. 1550 - 1561
参考文献
Journal of Medicinal Chemistry, , vol. 31, # 5 p. 944 - 948