双(4-氯苯基)二硒化物合成路线 （共 39 条）
反应条件
N,N-bis(trimethylsilyl)-N-chloroamine in tetrachloromethane
T=15 - 20°C; 0.5 h;
参考文献
Derkach, N.Ya.; Lyapina, T.V.; Levchenko, E.S.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 536 - 540
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 3 p. 622 - 627
反应条件
iodine in methanol
T=20°C; 5.5 h;
参考文献
Movassagh, Barahman; Moradi, Mona
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 1 p. 154 - 157
反应条件
selenium; samarium diiodide in tetrahydrofuran; N,N-dimethyl-formamide
参考文献
Zhang; Jia; Zhou
Synthetic Communications, 1994 , vol. 24, # 9 p. 1247 - 1252
反应条件
in N,N-dimethyl-formamide
T=70 - 80°C; 4 h;
参考文献
Liu; Chen
Synthetic Communications, 1993 , vol. 23, # 19 p. 2673 - 2676
反应条件
selenium in diethyl ether
参考文献
Sharpless,K.B.; Young,M.W.
Journal of Organic Chemistry, 1975 , vol. 40, p. 947 - 949
反应条件
1: 2.4 g / N-methylmorpholine / CH2Cl2 / 1.5 h / -10 °C
2: 25 mg / α,α'-azobisisobutyronitrile / toluene / Heating; Irradiation
View Scheme
参考文献
Brooks, Gerald; Hunt, Eric
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2513 - 2518
反应条件
in dichloromethane
T=25°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Schmid, George H.; Garratt, Dennis G.
Tetrahedron, 1985 , vol. 41, # 21 p. 4787 - 4792
参考文献
Challenger; Peters; Halevy
Journal of the Chemical Society, 1926 , p. 1654
反应条件
hydrogenchloride; zinc
参考文献
Challenger; Peters
Journal of the Chemical Society, 1928 , p. 1370
反应条件
1: Diazotization.Behandeln mit Kupfer(I)-chlorid in Salzsaeure
2: alcoholic KOH-solution
View Scheme
参考文献
Challenger; Peters; Halevy
Journal of the Chemical Society, 1926 , p. 1654
